Table 1.
13C-NMR data of friedelane-type pentacyclic triterpenoids isolated from Celastraceae species (2001–2021).
| C | F1 | F2 | F3 | F4 a | F6 b | F7 | F8 b | F9 | F10 | F11 |
|---|---|---|---|---|---|---|---|---|---|---|
| 1 | 25.0 | 22.3 | 22.3 | 22.3 | 22.8 | 22.3 | 202.8 | 22.2 | 202.4 | 22.8 |
| 2 | 41.6 | 41.4 | 41.2 | 41.4 | 42.7 | 41.5 | 60.6 | 41.4 | 60.4 | 41.9 |
| 3 | 213.3 | 212.7 | 212.3 | 212.7 | 211.9 | 213.0 | 204.0 | 213.0 | 203.8 | 212.1 |
| 4 | 52.1 | 58.1 | 58.0 | 58.1 | 57.8 | 58.2 | 58.9 | 58.1 | 58.6 | 58.3 |
| 5 | 43.1 | 41.8 | 41.8 | 41.9 | 42.4 | 42.0 | 38.1 | 42.0 | 37.4 | 42.4 |
| 6 | 42.2 | 41.1 | 40.8 | 41.2 | 41.7 | 41.3 | 41.5 | 41.1 | 40.2 | 41.5 |
| 7 | 17.9 | 18.3 | 18.4 | 18.1 | 22.7 | 20.0 | 20.4 | 18.3 | 17.9 | 18.9 |
| 8 | 52.8 | 51.3 | 52.0 | 52.9 | 54.4 | 53.5 | 52.4 | 49.9 | 48.8 | 50.8 |
| 9 | 44.1 | 38.3 | 38.1 | 38.2 | 38.0 | 37.8 | 37.1 | 37.4 | 36.6 | 38.0 |
| 10 | 60.1 | 59.3 | 59.1 | 59.4 | 59.8 | 59.4 | 72.3 | 59.5 | 71.5 | 59.8 |
| 11 | 76.9 | 47.0 | 47.3 | 47.4 | 37.1 | 35.6 | 34.9 | 34.9 | 33.7 | 35.6 |
| 12 | 42.0 | 72.1 | 71.2 | 72.7 | 31.6 | 31.2 | 29.9 | 29.3 | 29.1 | 30.4 |
| 13 | 41.1 | 44.8 | 45.7 | 45.3 | 41.0 | 40.6 | 39.7 | 39.9 | 39.3 | 39.9 |
| 14 | 38.2 | 41.1 | 40.8 | 40.4 | 46.8 | 44.1 | 42.9 | 39.2 | 38.8 | 40.2 |
| 15 | 32.4 | 31.6 | 50.3 | 33.4 | 75.5 | 74.6 | 31.3 | 36.8 | 38.7 | 40.2 |
| 16 | 35.9 | 35.9 | 218.3 | 36.1 | 48.4 | 48.4 | 78.1 | 74.3 | 75.5 | 75.7 |
| 17 | 30.0 | 31.3 | 45.7 | 30.8 | 30.9 | 30.2 | 35.0 | 41.0 | 37.0 | 37.7 |
| 18 | 42.5 | 44.3 | 45.4 | 44.2 | 42.6 | 41.6 | 45.5 | 41.7 | 45.6 | 46.66 |
| 19 | 35.4 | 31.7 | 38.5 | 38.4 | 32.2 | 35.6 | 35.7 | 33.7 | 33.8 | 34.3 |
| 20 | 28.1 | 33.3 | 27.8 | 28.4 | 28.4 | 28.1 | 28.1 | 28.0 | 27.7 | 28.6 |
| 21 | 32.7 | 29.9 | 31.5 | 32.7 | 36.2 | 31.9 | 31.8 | 33.8 | 33.2 | 35.0 |
| 22 | 39.2 | 38.1 | 30.7 | 39.6 | 39.5 | 38.7 | 34.9 | 19.8 | 26.2 | 27.8 |
| 23 | 6.9 | 6.8 | 6.8 | 6.8 | 7.2 | 6.8 | 7.3 | 6.7 | 7.0 | 7.5 |
| 24 | 14.8 | 14.6 | 14.6 | 14.6 | 14.4 | 14.5 | 15.8 | 14.7 | 15.7 | 15.1 |
| 25 | 12.9 | 19.2 | 18.7 | 19.3 | 16.9 | 17.9 | 18.2 | 19.2 | 18.8 | 19.4 |
| 26 | 20.1 | 18.7 | 20.5 | 20.5 | 65.8 | 14.0 | 63.2 | 16.5 | 16.8 | 17.7 |
| 27 | 19.5 | 11.6 | 9.0 | 11.6 | 19.7 | 18.7 | 20.9 | 19.7 | 19.1 | 20.0 |
| 28 | 32.0 | 31.7 | 27.3 | 31.8 | 32.7 | 32.6 | 25.9 | 71.3 | 29.9 | 31.0 |
| 29 | 31.7 | 71.6 | 31.3 | 34.9 | 35.7 | 30.9 | 37.8 | 37.0 | 31.8 | 32.7 |
| 30 | 35.0 | 29.2 | 35.0 | 31.9 | 31.0 | 35.6 | 30.4 | 31.8 | 36.2 | 36.9 |
| C=O | 171.3 | |||||||||
| OCH3 | 21.3 | |||||||||
| Ref | [35] | [36] | [37] | [38] | [39] | [40] | [41] | [42] | [43] | [44] |
| C | F12 a | F13 | F14 b | F15 a | F16 | F17 | F18 | F19 | F20 | F21 |
| 1 | 21.7 | 22.2 | 22.3 | 68.8 | 75.8 | 74.0 | 71.4 | 202.7 | 22.3 | 22.3 |
| 2 | 40.9 | 41.4 | 41.6 | 51.9 | 35.0 | 30.1 | 52.7 | 60.6 | 41.5 | 41.3 |
| 3 | 211.1 | 212.8 | 212.5 | 210.4 | 212.3 | 213.2 | 211.3 | 204.1 | 213.2 | 212.7 |
| 4 | 57.4 | 58.0 | 58.3 | 57.5 | 55.9 | 53.3 | 59.1 | 59.1 | 58.2 | 58.1 |
| 5 | 41.5 | 42.1 | 42.3 | 39.4 | 43.3 | 42.7 | 43.9 | 37.8 | 42.0 | 41.8 |
| 6 | 40.5 | 41.1 | 41.4 | 41.8 | 41.8 | 41.2 | 34.3 | 40.6 | 41.2 | 40.2 |
| 7 | 18.0 | 18.4 | 18.6 | 17.8 | 17.9 | 18.2 | 18.8 | 18.1 | 18.0 | 21.2 |
| 8 | 53.0 | 53.3 | 53.5 | 53.4 | 53.8 | 53.0 | 53.9 | 50.6 | 51.2 | 44.7 |
| 9 | 36.9 | 37.4 | 37.6 | 36.6 | 42.0 | 36.9 | 38.6 | 37.3 | 37.5 | 37.9 |
| 10 | 58.7 | 59.3 | 59.7 | 64.8 | 57.4 | 52.4 | 62.6 | 71.9 | 59.5 | 59.0 |
| 11 | 35.1 | 35.6 | 35.8 | 37.0 | 30.2 | 35.9 | 35.7 | 34.2 | 35.3 | 36.8 |
| 12 | 30.0 | 30.7 | 30.8 | 29.9 | 31.0 | 30.5 | 30.4 | 29.8 | 30.2 | 33.9 |
| 13 | 39.6 | 40.1 | 39.3 | 39.4 | 39.8 | 39.8 | 39.8 | 38.8 | 39.0 | 47.5 |
| 14 | 38.8 | 39.1 | 40.1 | 39.3 | 37.5 | 38.4 | 38.5 | 38.7 | 38.8 | 56.3 |
| 15 | 44.7 | 44.3 | 44.4 | 33.2 | 32.7 | 32.1 | 32.7 | 30.5 | 30.4 | 213.3 |
| 16 | 75.7 | 74.4 | 75.6 | 36.0 | 36.0 | 35.4 | 36.2 | 35.9 | 36.1 | 53.8 |
| 17 | 40.5 | 36.4 | 32.1 | 30.4 | 29.9 | 30.0 | 30.2 | 32.5 | 32.5 | 34.0 |
| 18 | 39.9 | 44.1 | 44.8 | 41.9 | 42.7 | 42.7 | 43.0 | 44.2 | 44.3 | 45.3 |
| 19 | 29.3 | 30.4 | 35.8 | 30.8 | 35.3 | 28.9 | 35.5 | 36.0 | 35.9 | 38.9 |
| 20 | 32.7 | 33.1 | 28.0 | 33.2 | 28.1 | 33.4 | 28.2 | 34.3 | 34.4 | 28.0 |
| 21 | 27.7 | 27.5 | 32.1 | 27.8 | 32.7 | 28.2 | 33.0 | 74.3 | 74.3 | 71.7 |
| 22 | 29.5 | 36.4 | 36.0 | 39.7 | 39.3 | 28.1 | 39.3 | 47.0 | 47.0 | 46.3 |
| 23 | 6.4 | 6.9 | 6.8 | 7.1 | 6.7 | 6.9 | 6.9 | 7.3 | 6.8 | 6.8 |
| 24 | 14.0 | 14.6 | 14.7 | 16.0 | 14.7 | 14.3 | 17.4 | 16.0 | 14.6 | 14.9 |
| 25 | 17.5 | 18.1 | 18.2 | 18.4 | 63.0 | 17.9 | 19.2 | 18.2 | 17.7 | 18.9 |
| 26 | 21.1 | 20.1 | 20.1 | 18.6 | 20.1 | 20.0 | 20.2 | 17.8 | 18.2 | 15.4 |
| 27 | 19.3 | 21.4 | 21.5 | 21.0 | 18.6 | 18.7 | 18.7 | 19.3 | 19.3 | 12.1 |
| 28 | 66.7 | 25.4 | 24.9 | 32.1 | 32.2 | 32.2 | 32.2 | 33.1 | 33.2 | 31.5 |
| 29 | 74.0 | 74.4 | 30.8 | 74.5 | 35.0 | 28.9 | 31.8 | 24.9 | 31.9 | 31.4 |
| 30 | 25.4 | 25.7 | 35.5 | 25.9 | 31.7 | 72.0 | 34.9 | 31.8 | 24.9 | 33.8 |
| Ref | [45] | [46] | [27] | [45] | [47] | [48] | [48] | [49] | [50] | [51] |
| C | F22 | F23 | F24 | F25 | F26 | F27 | F28 b | F29 | F30 | F31 |
| 1 | 22.4 | 202.8 | 24.7 | 24.6 | 202.8 | 22.5 | 22.4 | 22.3 | 202.7 | 22.1 |
| 2 | 41.6 | 60.5 | 42.6 | 42.5 | 60.6 | 41.6 | 41.6 | 41.5 | 60.6 | 41.3 |
| 3 | 213.2 | 230.7 | 212.9 | 212.8 | 204.1 | 213.3 | 211.7 | 212.9 | 204.1 | 213.6 |
| 4 | 58.4 | 59.7 | 58.5 | 58.5 | 58.9 | 58.4 | 57.9 | 58.3 | 59.0 | 57.8 |
| 5 | 42.4 | 37.5 | 42.4 | 42.4 | 38.1 | 42.3 | 42.1 | 42.1 | 37.2 | 41.9 |
| 6 | 41.4 | 38.5 | 41.8 | 41.7 | 41.7 | 41.5 | 41.2 | 41.4 | 40.6 | 41.0 |
| 7 | 18.4 | 17.0 | 17.9 | 18.0 | 20.4 | 18.6 | 18.4 | 18.3 | 18.0 | 18.1 |
| 8 | 53.4 | 45.2 | 53.7 | 53.9 | 52.0 | 53.8 | 53.2 | 53.5 | 51.5 | 52.2 |
| 9 | 37.6 | 37.1 | 42.0 | 42.0 | 37.1 | 37.6 | 37.5 | 37.5 | 37.8 | 37.3 |
| 10 | 59.6 | 69.0 | 60.7 | 60.7 | 72.4 | 59.7 | 59.2 | 59.6 | 71.9 | 59.1 |
| 11 | 35.8 | 35.8 | 29.9 | 30.0 | 35.0 | 37.8 | 35.7 | 35.5 | 33.4 | 35.3 |
| 12 | 30.8 | 26.5 | 31.2 | 31.4 | 29.9 | 24.1 | 30.5 | 30.0 | 29.7 | 29.9 |
| 13 | 39.8 | 38.1 | 39.7 | 39.9 | 39.7 | 45.4 | 40.1 | 39.6 | 39.2 | 39.1 |
| 14 | 38.4 | 40.0 | 37.7 | 37.9 | 42.0 | 38.4 | 38.2 | 38.4 | 39.1 | 38.0 |
| 15 | 32.5 | 34.7 | 32.7 | 33.0 | 20.1 | 32.2 | 29.5 | 31.1 | 31.2 | 31.3 * |
| 16 | 38.8 | 36.8 | 36.0 | 35.0 | 35.3 | 36.2 | 32.6 | 29.2 | 29.0 | 29.0 |
| 17 | 30.0 | 30.8 | 30.1 | 33.1 | 30.4 | 30.3 | 36.6 | 35.1 | 35.1 | 35.1 |
| 18 | 42.8 | 44.0 | 42.7 | 41.9 | 43.5 | 43.3 | 39.0 | 38.9 | 39.3 | 39.2 |
| 19 | 36.0 | 35.4 | 35.3 | 37.0 | 35.4 | 37.1 | 29.8 | 31.5 | 34.4 | 34.4 |
| 20 | 33.9 | 28.3 | 28.1 | 42.7 | 28.3 | 28.5 | 33.6 | 33.3 | 28.1 | 27.9 |
| 21 | 75.8 | 32.5 | 32.7 | 218.7 | 32.9 | 32.6 | 29.2 | 30.2 | 31.4 | 31.4 * |
| 22 | 48.6 | 38.9 | 39.2 | 55.0 | 39.1 | 40.1 | 33.0 | 28.3 | 34.3 | 33.2 |
| 23 | 6.9 | 7.5 | 7.0 | 7.0 | 7.3 | 7.1 | 7.2 | 6.8 | 7.3 | 6.7 |
| 24 | 14.8 | 15.7 | 14.7 | 14.7 | 15.7 | 14.9 | 14.7 | 14.7 | 15.9 | 14.5 |
| 25 | 18.0 | 67.1 | 63.0 | 62.7 | 17.8 | 18.2 | 18.0 | 18.2 | 18.1 | 18.0 |
| 26 | 20.8 | 69.9 | 20.1 | 20.9 | 64.0 | 22.3 | 20.1 | 18.6 | 19.1 | 18.9 |
| 27 | 18.9 | 19.3 | 18.5 | 18.4 | 19.7 | 63.4 | 19.0 | 19.1 | 19.2 | 19.1 |
| 28 | 34.5 | 30.0 | 32.1 | 33.6 | 31.7 | 32.8 | 67.1 | 69.0 | 68.0 | 67.0 |
| 29 | 34.9 | 31.4 | 35.0 | 28.8 | 34.5 | 35.8 | 73.6 | 28.6 | 34.2 | 32.9 |
| 30 | 24.1 | 35.1 | 31.7 | 25.0 | 32.0 | 30.6 | 27.5 | 73.4 | 32.8 | 34.2 |
| Ref | [52] | [53] | [48] | [54] | [41] | [55] | [56] | [57] | [58] | [57] |
| C | F32 | F34 | F35 | F36 | F37 | F38 | F39c | F40 | F41 | F42 |
| 1 | 22.7 | 22.2 | 22.5 | 25.9 | 32.4 | 31.7 | 28.2 | 24.8 | 202.7 | 22.3 |
| 2 | 41.4 | 41.3 | 41.6 | 75.4 | 76.9 | 74.4 | 71.0 | 42.6 | 60.6 | 41.5 |
| 3 | 213.4 | 212.2 | 212.8 | 105.6 | 212.0 | 209.7 | 199.6 | 212.3 | 204.1 | 212.9 |
| 4 | 58.6 | 57.9 | 58.6 | 47.4 | 52.7 | 52.4 | 127.1 | 58.6 | 59.1 | 58.3 |
| 5 | 42.3 | 42.0 | 42.4 | 46.8 | 42.7 | 54.2 | 158.8 | 42.3 | 37.8 | 42.1 |
| 6 | 41.9 | 40.8 | 41.7 | 33.3 | 40.8 | 36.7 | 30.4 | 41.6 | 40.6 | 41.4 |
| 7 | 18.4 | 18.5 | 18.5 | 19.2 | 17.5 | 19.4 | 20.3 | 18.2 | 18.0 | 18.3 |
| 8 | 53.2 | 52.3 | 53.7 | 49.8 | 52.7 | 49.6 | 47.3 | 54.0 | 52.0 | 53.1 |
| 9 | 38.0 | 37.5 | 37.8 | 37.1 | 38.0 | 37.5 | 37.2 | 41.1 | 37.2 | 37.5 |
| 10 | 59.6 | 59.0 | 59.9 | 53.2 | 52.7 | 55.7 | 51.8 | 60.3 | 71.9 | 59.6 |
| 11 | 35.7 | 35.2 | 36.0 | 34.3 | 35.6 | 34.5 | 32.4 | 30.1 | 34.5 | 35.7 |
| 12 | 31.0 | 28.9 | 30.8 | 29.0 | 30.2 | 29.4 | 28.9 | 30.7 | 30.1 | 29.4 |
| 13 | 37.6 | 39.0 | 38.6 | 39.2 | 39.4 | 40.2 | 39.2 | 39.9 | 39.6 | 39.9 |
| 14 | 39.3 | 40.6 | 40.3 | 39.1 | 38.9 | 39.4 | 39.5 | 37.9 | 38.3 | 38.2 |
| 15 | 28.6 | 50.2 | 33.0 | 29.1 | 32.7 | 28.3 | 27.9 | 33.1 | 32.1 | 32.2 |
| 16 | 32.8 | 218.4 | 36.2 | 36.2 | 36.5 | 29.6 | 35.1 | 34.9 | 35.8 | 29.7 |
| 17 | 48.6 | 45.7 | 30.8 | 30.1 | 29.8 | 44.8 | 37.7 | 33.0 | 30.0 | 30.0 |
| 18 | 35.9 | 43.2 | 42.3 | 44.5 | 42.4 | 45.4 | 43.4 | 41.8 | 42.6 | 42.9 |
| 19 | 29.8 | 30.1 | 39.8 | 30.4 | 35.0 | 31.6 | 31.3 | 36.9 | 29.4 | 30.6 |
| 20 | 33.7 | 32.7 | 33.4 | 40.6 | 27.8 | 41.4 | 41.9 | 42.7 | 33.4 | 33.4 |
| 21 | 28.0 | 27.0 | 30.0 | 30.0 | 32.0 | 214.2 | 213.7 | 218.7 | 28.1 | 28.3 |
| 22 | 33.7 | 31.1 | 28.1 | 36.6 | 40.8 | 77.5 | 53.3 | 55.0 | 38.1 | 39.9 |
| 23 | 7.2 | 6.9 | 7.0 | 7.1 | 6.3 | 7.9 | 10.7 | 7.0 | 7.3 | 6.8 |
| 24 | 15.0 | 14.6 | 14.9 | 72.4 | 13.8 | 174.2 | 14.8 | 16.0 | 14.7 | |
| 25 | 17.5 | 17.2 | 18.1 | 16.7 | 17.9 | 16.8 | 17.0 | 65.1 | 18.1 | 18.0 |
| 26 | 20.5 | 20.3 | 18.6 | 16.2 | 18.4 | 15.5 | 15.0 | 21.5 | 20.0 | 18.6 |
| 27 | 19.2 | 15.9 | 20.9 | 17.5 | 19.9 | 19.4 | 17.9 | 18.6 | 18.6 | 19.9 |
| 28 | 208.9 | 27.4 | 32.3 | 31.9 | 32.1 | 25.4 | 32.3 | 33.8 | 32.1 | 32.2 |
| 29 | 24.4 | 74.1 | 75.0 | 179.4 | 31.7 | 28.8 | 28.9 | 29.0 | ||
| 30 | 74.7 | 25.8 | 26.1 | 32.1 | 34.7 | 15.0 | 14.7 | 25.0 | 72.0 | 72.1 |
| OCH3 | 51.7 | |||||||||
| C=O | 166.8 | |||||||||
| Iso | 130.2 | |||||||||
| Orto | 129.5 | |||||||||
| Meta | 128.6 | |||||||||
| Para | 133.1 | |||||||||
| Ref | [48] | [46] | [59] | [48] | [60] | [61] | [62] | [54] | [49] | [57] |
| C | F43 | F44 | F45 | F47 | F49 | F50 | F51 | F52 | F53 | F54 |
| 1 | 31.3 | 200.5 | 27.6 | 22.2 | 22.3 | 39.0 | 36.1 | 26.7 | 26.7 | 210.9 |
| 2 | 193.1 | 102.6 | 41.2 | 41.5 | 41.5 | 211.4 | 211.7 | 72.7 | 73.2 | 53.9 |
| 3 | 146.5 | 175.5 | 213.0 | 213.0 | 213.0 | 77.2 | 77.0 | 106.3 | 106.8 | 75.4 |
| 4 | 126.9 | 49.9 | 57.9 | 58.2 | 58.2 | 54.8 | 54.6 | 45.6 | 45.7 | 50.0 |
| 5 | 54.7 | 41.6 | 41.7 | 42.1 | 42.1 | 38.0 | 38.1 | 52.8 | 47.0 | 44.5 |
| 6 | 30.7 | 41.1 | 40.7 | 41.2 | 41.3 | 41.1 | 40.7 | 72.8 | 33.6 | 42.7 |
| 7 | 18.4 | 17.6 | 17.8 | 18.0 | 18.2 | 17.3 | 17.6 | 30.4 | 19.2 | 18.2 |
| 8 | 49.4 | 52.3 | 51.5 | 52.8 | 50.4 | 53.8 | 53.2 | 46.5 | 49.7 | 53.2 |
| 9 | 37.0 | 37.1 | 37.4 | 37.1 | 37.5 | 41.8 | 37.7 | 37.0 | 37.0 | 37.2 |
| 10 | 55.8 | 68.7 | 59.0 | 59.2 | 59.6 | 60.8 | 60.5 | 52.7 | 52.6 | 71.8 |
| 11 | 33.1 | 35.3 | 34.8 | 35.4 | 35.2 | 29.5 | 35.1 | 34.0 | 34.1 | 35.2 |
| 12 | 29.2 | 30.4 | 30.4 | 30.6 | 30.5 | 30.5 | 20.3 | 29.7 | 29.0 | 30.9 |
| 13 | 39.2 | 39.4 | 37.5 | 38.7 | 39.3 * | 39.7 | 39.7 | 39.2 | 39.1 | 40.6 |
| 14 | 39.1 | 38.3 | 38.4 | 37.6 | 39.4 * | 38.2 | 38.4 | 38.9 | 49.1 | 38.8 |
| 15 | 28.9 | 32.5 | 32.6 | 32.4 | 30.0 | 32.7 | 32.4 | 29.1 | 29.0 | 33.3 |
| 16 | 36.0 | 36.0 | 29.3 | 34.9 | 36.2 | 35.9 | 36.0 | 36.1 | 36.2 | 36.6 |
| 17 | 30.1 | 29.9 | 42.4 | 47.7 | 30.2 | 30.0 | 30.0 | 30.5 | 30.1 | 31.1 |
| 18 | 44.4 | 42.7 | 38.5 | 36.4 | 44.6 | 42.6 | 42.9 | 44.5 | 44.5 | 42.6 |
| 19 | 30.4 | 35.1 | 34.1 | 35.4 | 29.2 | 35.3 | 35.4 | 30.1 | 30.4 | 30.7 |
| 20 | 40.5 | 28.2 | 32.8 | 28.3 | 40.6 | 28.1 | 28.2 | 40.5 | 40.5 | 34.0 |
| 21 | 29.9 | 32.8 | 31.0 | 32.4 | 29.6 | 32.7 | 32.8 | 30.0 | 30.0 | 28.7 |
| 22 | 36.5 | 39.3 | 22.0 | 28.0 | 36.6 | 39.2 | 39.3 | 36.5 | 36.4 | 40.5 |
| 23 | 10.6 | 8.5 | 6.6 | 6.8 | 6.8 | 10.9 | 10.8 | 9.9 | 6.9 | 12.4 |
| 24 | 194.9 | 15.1 | 14.3 | 14.6 | 14.6 | 14.0 | 14.2 | 64.6 | 72.2 | 18.4 |
| 25 | 17.4 | 18.1 | 17.0 | 17.2 | 17.5 | 63.7 | 17.4 | 16.5 | 16.7 | 19.0 |
| 26 | 15.9 | 20.4 | 19.0 | 20.0 | 18.5 | 20.3 | 20.2 | 16.1 | 16.1 | 21.3 |
| 27 | 17.2 | 18.7 | 16.1 | 18.8 | 16.1 | 18.5 | 18.5 | 1.4 | 17.4 | 19.1 |
| 28 | 31.8 | 32.0 | 177.0 | 209.1 | 31.9 | 32.2 | 31.1 | 31.8 | 31.8 | 32.7 |
| 29 | 179.1 | 35.0 | 26.7 | 34.5 | 179.3 | 35.0 | 31.8 | 179.1 | 179.1 | 74.7 |
| 30 | 31.9 | 31.7 | 79.7 | 29.4 | 31.9 | 31.7 | 35.0 | 32.0 | 32.0 | 26.9 |
| OCH3 | 51.5 | 55.6 | 51.5 | |||||||
| Ref | [63] | [64] | [48] | [65] | [66] | [47] | [67] | [68] | [48] | [69] |
| C | F55 | F56 | F57 | F59 b | F60 | F61 | F62 | F63 | F64 b | F65 c |
| 1 | 21.7 | 29.6 | 146.3 | 35.6 | 21.9 | 22.3 | 22.4 | 74.0 | 28.7 | 26.6 |
| 2 | 37.1 | 72.4 | 130.1 | 41.1 | 41.2 | 41.7 | 41.7 | 29.7 | 74.2 | 68.5 |
| 3 | 216.6 | 202.3 | 200.9 | 212.4 | 212.4 | 212.8 | 212.7 | 231.2 | 108.1 | 71.2 |
| 4 | 58.7 | 129.5 | 57.7 | 58.1 | 58.2 | 58.8 | 58.8 | 53.3 | 46.8 | 42.8 |
| 5 | 39.9 | 157.8 | 49.1 | 42.5 | 42.6 | 41.3 | 41.3 | 42.7 | 47.5 | 49.0 |
| 6 | 37.4 | 65.4 | 77.2 | 50.4 | 52.2 | 49.0 | 48.9 | 41.2 | 34.0 | 37.2 |
| 7 | 17.7 | 29.9 | 28.7 | 69.2 | 68.6 | 68.4 | 68.3 | 18.1 | 19.7 | 19.0 |
| 8 | 53.5 | 40.9 | 48.2 | 58.2 | 58.6 | 52.9 | 52.6 | 53.1 | 50.4 | 49.2 |
| 9 | 37.0 | 38.5 | 36.7 | 38.8 | 39.0 | 37.2 | 37.6 | 36.9 | 37.5 | 44.0 |
| 10 | 49.4 | 48.9 | 60.3 | 59.3 | 58.9 | 60.0 | 59.8 | 52.4 | 53.3 | 50.0 |
| 11 | 35.7 | 33.4 | 45.4 | 36.0 | 35.9 | 37.6 | 31.2 | 32.7 | 34.7 | 33.8 |
| 12 | 30.5 | 29.5 | 69.3 | 29.9 | 29.6 | 30.5 | 37.5 | 29.5 | 29.5 | 28.8 |
| 13 | 39.7 | 39.3 | 40.0 | 40.3 | 40.3 | 40.4 | 39.5 | 39.7 | 39.6 | 39.6 |
| 14 | 38.3 | 40.6 | 45.6 | 44.2 | 40.0 | 39.1 | 44.9 | 38.0 | 39.3 | 38.8 |
| 15 | 32.4 | 28.3 | 49.6 | 27.0 | 29.5 | 32.4 | 32.8 | 30.2 | 29.7 | 27.8 |
| 16 | 36.0 | 29.8 | 214.2 | 35.5 | 38.3 | 35.8 | 29.1 | 35.3 | 36.7 | 28.9 |
| 17 | 30.0 | 45.2 | 47.1 | 30.1 | 30.4 | 30.5 | 38.3 | 30.0 | 30.5 | 36.4 |
| 18 | 42.7 | 45.8 | 44.7 | 43.3 | 42.3 | 41.6 | 38.0 | 42.4 | 44.8 | 45.0 |
| 19 | 35.3 | 32.0 | 39.6 | 21.9 | 35.3 | 29.6 | 35.1 | 31.3 | 30.9 | 30.9 |
| 20 | 28.1 | 41.7 | 42.3 | 28.3 | 33.5 | 33.1 | 28.5 | 40.2 | 40.7 | 40.8 |
| 21 | 32.7 | 214.1 | 218.1 | 32.4 | 27.9 | 27.9 | 35.9 | 28.2 | 30.5 | 213.2 |
| 22 | 39.2 | 78.1 | 47.2 | 39.2 | 36.1 | 39.4 | 32.5 | 38.2 | 37.4 | 76.7 |
| 23 | 13.5 | 11.1 | 9.8 | 6.9 | 6.9 | 6.9 | 6.9 | 6.8 | 8.4 | 11.3 |
| 24 | 23.1 | 8.7 | 15.9 | 15.9 | 16.1 | 16.1 | 14.4 | 72.1 | 176.5 | |
| 25 | 18.0 | 17.0 | 19.6 | 18.8 | 18.9 | 19.0 | 18.8 | 17.5 | 16.9 | 15.2 |
| 26 | 20.4 | 15.8 | 19.9 | 64.2 | 13.1 | 21.8 | 21.4 | 20.9 | 16.8 | 17.3 |
| 27 | 18.7 | 19.3 | 8.7 | 20.1 | 20.8 | 18.3 | 18.5 | 17.7 | 18.1 | 18.6 |
| 28 | 32.1 | 25.9 | 29.1 | 31.2 | 31.8 | 32.1 | 179.2 | 32.0 | 32.1 | 25.5 |
| 29 | 35.0 | 28.4 | 34.7 | 29.1 | 74.5 | 34.4 | 31.8 | 181.3 | ||
| 30 | 31.7 | 15.4 | 24.4 | 31.1 | 71.3 | 26.0 | 29.6 | 183.1 | 32.3 | 14.9 |
| Ref | [70] | [71] | [72] | [39] | [73] | [48] | [48] | [48] | [74] | [75] |
| C | F66 | F67 + | F68 | F69 b | F70 b | F71 | F72 | F73 | F74 | F75 b |
| 1 | 30.8 | 28.2 | 32.6 | 30.9 | 39.0 | 22.3 | 22.2 | 22.3 | 36.5 | 20.3 |
| 2 | 74.1 | 76.5 | 75.0 | 193.5 | 194.6 | 41.5 | 42.0 | 41.5 | 212.3 | 38.9 |
| 3 | 213.3 | 208.1 | 212.4 | 149.0 | 144.2 | 213.2 | 213.3 | 213.3 | 77.3 | 105.9 |
| 4 | 52.7 | 54.3 | 55.6 | 125.8 | 139.9 | 58.2 | 58.2 | 58.3 | 54.8 | 53.7 |
| 5 | 43.1 | 43.1 | 43.1 | 54.9 | 40.0 | 42.1 | 44.7 | 42.0 | 39.6 | 47.0 |
| 6 | 41.3 | 41.0 | 41.2 | 32.7 | 33.6 | 41.2 | 41.5 | 41.3 | 40.9 | 33.9 |
| 7 | 18.5 | 18.2 | 18.1 | 18.9 | 18.2 | 18.2 | 18.4 | 18.2 | 17.9 | 19.4 |
| 8 | 50.9 | 50.4 | 53.2 | 49.5 | 50.8 | 53.1 | 52.9 | 50.7 | 51.0 | 50.0 |
| 9 | 37.2 | 36.6 | 37.4 | 37.1 | 37.8 | 37.5 | 37.7 | 37.4 | 38.3 | 37.3 |
| 10 | 52.6 | 53.3 | 56.5 | 55.5 | 56.1 | 59.4 | 59.2 | 59.8 | 60.9 | 57.1 |
| 11 | 35.4 | 35.1 | 35.3 | 33.3 | 35.0 | 35.6 | 35.9 | 36.1 | 35.0 | 34.6 |
| 12 | 30.5 | 30.1 | 30.2 | 30.9 | 30.7 | 30.3 | 31.0 | 29.5 | 29.7 | 29.4 |
| 13 | 39.5 | 39.2 | 39.7 | 39.4 | 39.7 | 39.7 | 41.0 | 39.2 | 38.0 | 39.4 |
| 14 | 39.7 | 39.3 | 38.1 | 39.6 | 39.8 | 38.0 | 38.8 | 39.1 | 39.5 | 39.2 |
| 15 | 29.8 | 30.4 | 32.8 | 30.5 | 30.6 | 32.8 | 29.3 | 29.4 | 30.1 | 29.3 |
| 16 | 37.8 | 36.2 | 35.4 | 36.6 | 36.8 | 35.4 | 32.6 | 36.6 | 36.5 | 36.5 |
| 17 | 30.4 | 29.1 | 29.6 | 30.5 | 31.2 | 29.5 | 37.6 | 30.1 | 30.5 | 30.3 |
| 18 | 44.8 | 44.5 | 42.5 | 44.8 | 45.0 | 42.5 | 37.6 | 44.2 | 44.7 | 44.6 |
| 19 | 30.8 | 36.9 | 31.3 | 29.5 | 29.9 | 31.2 | 35.4 | 29.3 | 30.6 | 30.7 |
| 20 | 40.7 | 40.6 | 40.3 | 40.7 | 40.9 | 40.3 | 28.4 | 40.4 | 40.6 | 40.5 |
| 21 | 29.7 | 29.9 | 28.2 | 29.4 | 30.1 | 28.2 | 34.8 | 30.2 | 29.7 | 30.3 |
| 22 | 36.7 | 29.4 | 38.2 | 37.4 | 37.2 | 38.2 | 32.6 | 35.2 | 37.1 | 37.2 |
| 23 | 6.8 | 6.5 | 6.5 | 10.7 | 10.5 | 6.8 | 6.8 | 6.9 | 11.2 | 8.4 |
| 24 | 14.2 | 14.1 | 14.7 | 195.8 | 19.1 | 14.6 | 14.6 | 14.6 | 14.6 | 72.9 |
| 25 | 18.0 | 18.3 | 17.8 | 17.2 | 18.2 | 17.7 | 17.5 | 18.4 | 18.1 | 16.7 |
| 26 | 18.5 | 16.1 | 20.9 | 17.9 | 18.5 | 20.9 | 20.7 | 16.3 | 18.2 | 17.9 |
| 27 | 16.1 | 17.5 | 17.7 | 16.2 | 17.0 | 17.7 | 18.5 | 18.0 | 16.6 | 16.5 |
| 28 | 32.1 | 31.8 | 31.8 | 32.3 | 32.0 | 32.0 | 185.0 | 31.8 | 32.2 | 31.9 |
| 29 | 181.2 | 31.9 | 183.3 | 181.5 | 181.2 | 31.9 | 29.7 | 184.8 | 32.1 | 181.2 |
| 30 | 32.1 | 179.4 | 32.0 | 32.1 | 32.3 | 184.7 | 34.5 | 31.5 | 182.4 | 32.2 |
| COOCH3 | 179.4 | |||||||||
| COOCH3 | 51.6 | |||||||||
| COOCH3 | 169.8 | |||||||||
| COOCH3 | 21.2 | |||||||||
| Ref | [76] | [77] | [78] | [59] | [79] | [80] | [56] | [81] | [82] | [83] |
| C | F76 | F77 c | F79 | F80 | F81 | F82 | F83 | F84 | F85 | F86 |
| 1 | 19.3 | 26.6 | 22.4 | 16.0 | 148.2 | 202.7 | 202.8 | 22.2 | 22.3 | 22.3 |
| 2 | 36.3 | 67.6 | 41.7 | 35.4 | 130.4 | 60.6 | 60.6 | 40.8 | 41.1 | 41.4 |
| 3 | 71.9 | 83.1 | 212.7 | 73.0 | 201.5 | 204.0 | 204.2 | 212.1 | 212.1 | 213.1 |
| 4 | 52.9 | 43.3 | 58.8 | 49.4 | 57.6 | 59.0 | 59.1 | 57.9 | 58.1 | 58.2 |
| 5 | 37.4 | 48.6 | 41.3 | 38.0 | 43.7 | 37.8 | 37.8 | 42.2 | 42.2 | 42.0 |
| 6 | 40.9 | 33.3 | 48.9 | 41.9 | 39.5 | 40.5 | 40.6 | 41.0 | 41.0 | 40.5 |
| 7 | 17.4 | 18.7 | 68.3 | 17.7 | 18.1 | 18.1 | 18.1 | 18.4 | 18.6 | 21.3 |
| 8 | 52.6 | 49.6 | 52.9 | 53.7 | 51.5 | 52.4 | 52.2 | 53.0* | 53.1 | 45.3 |
| 9 | 37.0 | 36.8 | 37.6 | 37.3 | 36.8 | 37.2 | 37.2 | 55.5 | 43.8 | 37.2 |
| 10 | 59.6 | 52.2 | 59.8 | 61.5 | 61.9 | 71.8 | 71.9 | 53.1* | 59.3 | 59.3 |
| 11 | 35.6 | 33.7 | 31.1 | 35.8 | 34.4 | 34.5 | 34.6 | 214.2 | 51.4 | 34.4 |
| 12 | 30.9 | 28.7 | 37.8 | 30.9 | 28.8 | 30.3 | 30.2 | 51.2 | 214.2 | 29.4 |
| 13 | 37.8 | 38.6 | 39.5 | 40.1 | 39.0 | 39.7 | 39.5 | 44.0 | 55.5 | 42.4 |
| 14 | 38.6 | 38.6 | 44.6 | 38.5 | 40.5 | 38.1 | 38.2 | 43.8 | 44.0 | 54.2 |
| 15 | 32.3 | 29.4 | 32.8 | 32.8 | 49.8 | 32.7 | 32.4 | 31.6 | 35.6 | 214.9 |
| 16 | 29.2 | 35.9 | 29.2 | 36.1 | 218.7 | 35.0 | 35.9 | 36.1 | 36.2 | 54.0 |
| 17 | 44.5 | 29.7 | 38.4 | 30.7 | 45.3 | 33.2 | 30.0 | 29.6 | 29.7 | 33.5 |
| 18 | 37.6 | 44.0 | 38.4 | 42.0 | 43.9 | 41.8 | 42.7 | 36.4 | 36.6 | 44.0 |
| 19 | 34.5 | 29.7 | 35.1 | 29.9 | 35.4 | 37.0 | 35.3 | 35.4 | 31.7 | 34.9 |
| 20 | 28.2 | 40.6 | 28.5 | 33.3 | 27.6 | 42.8 | 28.2 | 28.3 | 28.4 | 27.9 |
| 21 | 35.1 | 29.4 | 35.8 | 28.0 | 31.6 | 218.8 | 32.8 | 33.0 | 33.1 | 33.8 |
| 22 | 32.2 | 36.3 | 32.4 | 39.7 | 30.7 | 55.0 | 39.3 | 38.9 | 39.1 | 38.6 |
| 23 | 9.6 | 14.3 | 6.9 | 11.8 | 6.7 | 7.3 | 7.3 | 6.8 | 6.9 | 6.8 |
| 24 | 14.3 | 96.5 | 16.1 | 16.6 | 13.7 | 16.0 | 16.0 | 14.5 | 14.6 | 15.0 |
| 25 | 17.4 | 16.3 | 18.8 | 18.4 | 19.1 | 17.8 | 18.0 | 18.1 | 18.2 | 17.4 |
| 26 | 20.3 | 16.1 | 21.7 | 20.8 | 19.8 | 21.3 | 20.3 | 19.0 | 19.9 | 14.7 |
| 27 | 18.3 | 17.2 | 18.5 | 18.7 | 16.2 | 18.5 | 18.7 | 19.8 | 19.1 | 18.9 |
| 28 | 183.7 | 31.7 | 183.3 | 32.3 | 27.4 | 33.5 | 32.0 | 31.8 | 31.9 | 32.2 |
| 29 | 29.5 | 179.6 | 34.3 | 75.0 | 35.2 | 28.8 | 31.8 | 31.7 | 31.8 | 33.3 |
| 30 | 34.2 | 31.6 | 29.7 | 26.0 | 31.1 | 25.0 | 35.0 | 34.2 | 34.3 | 33.4 |
| Ref | [48] | [84] | [48] | [69] | [45] | [52] | [85] | [86] | [35] | [51] |
| C | F87 | F88 | F89 | F90 | F91 b | F92 | F93 a | F94 | F95 | F96 |
| 1 | 22.2 | 21.6 | 22.2 | 18.6 | 17.0 | 16.0 | 16.2 | 41.3 | 27.8 | 31.4 |
| 2 | 41.4 | 40.8 | 41.4 | 35.4 | 40.3 | 35.5 | 36.1 | 41.6 | 170.4 | 193.2 |
| 3 | 212.5 | 210.6 | 212.8 | 72.0 | 74.7 | 72.0 | 71.6 | 213.0 | 177.0 | 146.5 |
| 4 | 58.2 | 57.8 | 58.1 | 49.4 | 491 | 49.4 | 49.6 | 59.5 | 47.3 | 127.0 |
| 5 | 42.1 | 47.0 | 42.0 | 38.3 | 41.4 | 37.9 | 38.1 | 42.2 | 38.9 | 54.7 |
| 6 | 41.0 | 56.9 | 41.2 | 41.9 | 36.0 | 41.8 | 42.0 | 35.6 | 34.5 | 30.6 |
| 7 | 18.6 | 210.2 | 18.1 | 17.5 | 19.3 | 17.7 | 17.7 | 30.7 | 17.1 | 18.3 |
| 8 | 52.4 | 63.4 | 53.0 | 52.9 | 53.8 | 53.2 | 53.3 | 53.4 | 52.0 | 48.7 |
| 9 | 37.7 | 42.4 | 37.4 | 43.9 | 36.8 | 37.1 | 37.2 | 37.5 | 35.3 | 37.0 |
| 10 | 59.4 | 59.0 | 59.4 | 62.3 | 61.6 | 61.5 | 61.6 | 58.2 | 46.1 | 56.0 |
| 11 | 35.4 | 35.5 | 35.5 | 76.6 | 36.5 | 35.5 | 35.7 | 22.4 * | 32.0 | 33.3 |
| 12 | 29.1 | 29.8 | 30.4 | 42.0 | 31.4 | 30.3 | 30.7 | 32.9 | 30.1 | 28.8 |
| 13 | 39.2 | 39.4 | 39.6 | 38.5 | 37.6 | 39.7 | 38.4 | 38.3 | 39.6 | 40.7 |
| 14 | 40.5 | 37.5 | 38.2 | 40.9 | 39.9 | 38.0 | 39.7 | 40.0 | 38.0 | 39.5 |
| 15 | 50.2 | 31.6 | 32.2 | 32.3 | 32.5 | 32.3 | 32.3 | 18.4 * | 32.3 | 28.2 |
| 16 | 218.8 | 36.3 | 35.9 | 36.0 | 35.6 | 32.0 | 35.9 | 37.1 | 35.7 | 35.9 |
| 17 | 45.3 | 30.1 | 29.9 | 30.0 | 30.7 | 36.1 | 30.0 | 42.8 | 30.0 | 31.4 |
| 18 | 44.0 | 41.8 | 42.8 | 42.6 | 43.6 | 38.5 | 42.9 | 42.0 | 42.6 | 45.3 |
| 19 | 35.5 | 34.9 | 35.2 | 35.7 | 35.6 | 29.3 | 35.4 | 35.1 | 35.2 | 29.8 |
| 20 | 27.6 | 28.0 | 28.0 | 28.1 | 28.8 | 33.1 | 28.2 | 33.3 | 28.1 | 149.1 |
| 21 | 31.7 | 32.8 | 32.7 | 32.8 | 32.9 | 28.4 | 32.9 | 218.8 | 32.6 | 30.7 |
| 22 | 30.8 | 38.6 | 39.2 | 39.2 | 39.0 | 28.7 | 39.3 | 55.1 | 39.1 | 38.0 |
| 23 | 6.8 | 6.8 | 6.7 | 12.1 | 14.8 | 11.9 | 12.1 | 6.9 | 12.5 | 10.7 |
| 24 | 14.7 | 15.1 | 14.5 | 16.7 | 65.8 | 16.5 | 16.6 | 17.9 | 20.6 | 194.9 |
| 25 | 17.3 | 18.2 | 17.8 | 13.5 | 18.4 | 18.3 | 18.3 | 14.8 | 72.6 | 18.1 |
| 26 | 20.3 | 19.2 | 18.5 | 19.9 | 18.9 | 20.0 | 20.1 | 33.6 | 20.2 | 15.1 |
| 27 | 16.2 | 19.4 | 20.1 | 19.5 | 20.8 | 18.8 | 18.7 | 21.4 | 18.5 | 17.9 |
| 28 | 27.4 | 32.1 | 32.0 | 32.0 | 33.6 | 66.7 | 32.1 | 18.6 | 32.1 | 31.4 |
| 29 | 31.1 | 31.8 | 31.7 | 35.0 | 35.6 | 73.8 | 35.0 | 25.1 | 35.0 | |
| 30 | 35.2 | 34.6 | 34.9 | 31.7 | 32.7 | 26.5 | 31.8 | 28.9 | 31.6 | 107.6 |
| Ref | [57] | [57] | [57] | [87] | [88] | [69] | [89] | [90] | [47] | [91] |
| C | F97C | F98 | F99 | F100 | F101 | F102 | F103 | |||
| 1 | 26.9 | 22.0 | 28.7 | 19.1 | 21.3 | 21.1 | 116.0 | |||
| 2 | 105.0 | 41.2 | 71.5 | 34.5 | 38.0 | 37.2 | 166.1 | |||
| 3 | 77.1 | 212.8 | 200.1 | 175.6 | 176.2 | 177.8 | ||||
| 4 | 47.7 | 57.9 | 127.7 | 36.1 | 35.8 | 36.2 | 197.9 | |||
| 5 | 44.6 | 41.9 | 159.2 | 36.8 | 37.5 | 37.9 | 135.5 | |||
| 6 | 30.1 | 41.0 | 30.9 | 38.8 | 38.7 | 39.0 | 136.0 | |||
| 7 | 18.6 | 18.0 | 20.8 | 18.0 | 17.9 | 18.2 | 118.6 | |||
| 8 | 48.1 | 53.1 | 47.7 | 52.6 | 52.1 | 53.1 | 163.3 | |||
| 9 | 37.5 | 37.2 | 37.6 | 42.9 | 38.8 | 39.1 | 39.2 | |||
| 10 | 52.1 | 59.2 | 52.3 | 58.2 | 59.6 | 59.9 | 165.9 | |||
| 11 | 33.3 | 35.3 | 33.1 | 84.1 | 34.7 | 35.3 | 31.2 | |||
| 12 | 28.8 | 29.8 | 29.5 | 37.6 | 29.5 | 30.3 | 29.2 | |||
| 13 | 40.2 | 38.0 | 39.5 | 40.7 | 39.0 | 39.7 | 38.3 | |||
| 14 | 39.1 | 39.6 | 40.0 | 37.9 | 37.9 | 38.4 | 47.6 | |||
| 15 | 28.3 | 32.3 | 28.1 | 32.1 | 31.1 | 32.4 | 28.5 | |||
| 16 | 29.6 | 35.5 | 29.7 | 35.9 | 29.0 | 36.1 | 36.6 | |||
| 17 | 44.8 | 30.1 | 44.9 | 30.0 | 35.0 | 30.1 | 30.4 | |||
| 18 | 45.6 | 41.6 | 45.3 | 42.6 | 39.3 | 43.0 | 44.6 | |||
| 19 | 31.7 | 30.3 | 31.7 | 35.3 | 34.3 | 35.4 | 31.1 | |||
| 20 | 41.5 | 31.4 | 41.3 | 28.1 | 27.8 | 28.2 | 40.4 | |||
| 21 | 213.9 | 27.7 | 214.0 | 32.7 | 33.2 | 32.9 | 29.7 | |||
| 22 | 77.4 | 38.8 | 77.2 | 39.2 | 31.3 | 39.3 | 34.4 | |||
| 23 | 16.1 | 6.6 | 11.2 | 7.7 | 7.3 | 7.6 | 18.1 | |||
| 24 | 175.3 | 14.4 | 22.1 | 19.2 | 19.5 | |||||
| 25 | 16.6 | 17.6 | 15.6 | 13.6 | 17.8 | 18.0 | 25.6 | |||
| 26 | 15.8 | 18.2 | 19.1 | 19.9 | 18.6 | 20.2 | 24.0 | |||
| 27 | 19.3 | 20.7 | 17.5 | 19.3 | 19.0 | 18.7 | 20.3 | |||
| 28 | 26.1 | 31.8 | 25.2 | 32.0 | 67.3 | 32.2 | 31.5 | |||
| 29 | 74.3 | 34.9 | 32.6 | 35.0 | 179.1 | |||||
| 30 | 15.6 | 25.9 | 14.8 | 31.7 | 33.9 | 31.9 | 32.8 | |||
| C=O | 161.2 | |||||||||
| OCH3 | 51.8 | |||||||||
| OCH3 | 51.8 | |||||||||
| Ref | [62] | [92] | [93] | [94] | [95] | [95] | [96] |
Ref: References; + 13C-NMR data of acetylated compound; * Values bearing the same superscript are interchangeable; Solvent: CDCl3; a CDCl3 + Pyridine-d5, b Pyridine-d5; c DMSO-d6; 13C-NMR data of some compounds were not found. In these cases, the reported identification was performed by comparison of other physical data: F5 [97], F33 [98], F46 (1H-NMR) [99], F48 (1H-NMR) [100], F58 (IR, MS) [101] and F78 (X-ray) [102].