. 2022 Jan 31;27(3):959. doi: 10.3390/molecules27030959

Table 6.

¹³C-NMR data of oleanane-type pentacyclic triterpenoids isolated from Celastraceae species (2001–2021).

C	O1	O2	O3	O4	O5	O6	O7	O8	O9 ^a	O10 ^a
1	38.7	32.8	41.1	40.3	33.8	39.3	40.3	40.3	39.0	72.3
2	33.8	26.6	32.8	34.4	25.5	27.3	34.4	34.2	34.2	35.5
3	216.2	75.9	217.4	218.0	76.1	78.6	218.2	217.8	215.9	72.3
4	47.5	37.4	47.7	47.7	37.5	39.0	47.8	47.7	47.6	40.1
5	54.7	48.2	54.9	55.5	48.8	55.0	55.4	55.3	54.5	47.8
6	18.7	17.5	19.7	19.8	18.3	18.2	19.8	19.7	19.2	17.8
7	30.5	31.1	32.8	33.9	33.2	33.1	32.7	32.6	30.9	32.8
8	40.6	40.7	41.9	42.9	43.3	43.0	43.2	43.2	41.7	45.2
9	50.1	50.4	55.5	50.4	51.2	51.6	48.7	48.5	52.8	53.8
10	36.2	36.6	37.6	37.7	38.3	38.1	37.6	37.5	36.3	42.1
11	52.5	57.0	67.9	76.3	75.9	75.8	81.7	82.0	132.3	200.9
12	57.0	52.9	125.5	121.6	122.5	121.5	122.3	121.2	131.3	128.6
13	87.3	87.9	149.0	149.3	148.3	149.7	150.8	152.8	84.9	169.7
14	41.2	41.3	43.2	42.0	41.8	41.7	42.0	42.3	44.2	44.0
15	26.7	26.7	26.4	26.2	26.1	26.1	26.3	27.9	25.7	26.7
16	21.2	21.6	26.0	26.8	28.1	26.6	28.1	26.6	26.0	26.5
17	43.8	43.7	32.3	32.4	34.8	32.3	34.9	33.1	41.9	32.5
18	49.6	49.1	46.7	47.2	46.3	46.8	46.5	47.0	51.1	47.6
19	37.8	32.5	46.3	46.4	46.7	46.3	46.9	46.7	32.4	45.2
20	31.5	36.8	31.0	31.1	36.3	31.1	36.5	31.1	36.7	31.0
21	34.3	29.7	34.6	34.7	73.9	34.5	74.0	34.6	30.9	34.5
22	27.0	27.7	36.8	36.9	45.2	36.8	45.2	36.9	30.6	36.7
23	25.9	28.0	26.7	26.7	28.6	28.0	26.7	26.9	26.2	28.8
24	21.1	21.8	21.5	21.5	22.4	15.4	21.6	21.5	21.0	16.2
25	16.4	17.0	16.2	16.4	16.7	18.0	16.4	18.0	17.3	18.0
26	18.7	20.1	17.9	18.1	18.2	16.8	18.2	16.2	19.4	19.1
27	19.8	18.1	26.1	25.2	25.2	25.1	24.7	24.7	19.6	23.6
28	179.2	179.1	28.4	28.5	28.4	28.3	28.5	28.5	77.1	28.8
29	33.2	26.6	33.0	33.2	28.9	33.1	29.1	33.2	28.9	33.0
30	23.6	65.7	23.6	23.6	16.9	23.5	17.0	23.6	65.0	23.5
OCH₃				53.7	53.7	53.7
Ref	[184]	[185]	[186]	[104]	[187]	[188]	[187]	[187]	[189]	[190]
C	O11	O12	O13	O14	O15	O16	O17	O18 ^b	O19 ^a	O20
1	39.6	39.4	39.3	40.0	38.1	39.8	48.6	47.6	47.7	46.6
2	33.8	34.2	34.2	34.5	24.0	34.0	69.1	69.6	68.7	69.0
3	218.1	217.7	217.8	217.5	80.3	218.3	83.1	85.9	85.7	84.0
4	47.0	47.5	47.5	48.1	37.5	47.2	39.3	44.3	43.9	39.3
5	54.6	55.4	55.3	55.7	55.0	54.8	55.5	57.3	56.5	55.4
6	19.4	19.7	19.6	19.1	18.8	19.6	17.7	19.8	19.2	18.4
7	33.7	32.2	32.1	32.3	32.2	33.7	34.0	34.3	33.5	33.1
8	40.6	39.9	39.7	45.2	39.6	40.6	43.5	40.9	40.0	39.4
9	50.1	46.9	46.8	61.3	47.2	50.4	56.8	49.2	48.3	47.6
10	36.7	36.7	36.7	37.0	38.0	36.8	40.1	39.2	38.3	38.3
11	21.3	23.8	23.7	199.3	23.3	21.5	72.3	25.1	24.2	23.6
12	25.7	123.6	122.4	128.2	123.1	26.0	211.1	124.6	122.4	124.5
13	37.6	142.5	143.8	168.9	142.6	38.9	82.4	144.4	144.4	140.5
14	43.6	41.9	41.8	43.8	41.8	43.2	45.3	42.5	42.1	42.6
15	27.3	25.6	26.0	26.1	25.2	27.3	22.6	30.3	29.1	24.4
16	36.3	23.6	28.2	30.9	18.0	36.8	30.5	27.9	23.1	25.3
17	36.9	39.6	35.0	37.3	31.7	34.5	33.6	47.0	47.0	35.3
18	142.9	48.0	46.7	43.0	46.1	147.5	49.0	45.0	41.8	43.5
19	127.7	41.4	47.0	45.5	40.0	124.7	38.5	82.3	46.2	33.9
20	40.0	151.6	36.3	31.3	42.6	28.0	31.4	35.9	30.8	39.6
21	73.1	69.1	74.0	34.1	36.6	27.9	34.1	29.4	34.0	39.9
22	43.5	45.9	45.3	21.8	75.2	37.3	39.0	33.1	32.2	83.2
23	26.6	26.6	26.5	21.7	23.8	26.8	28.7	23.8	24.2	28.7
24	20.7	21.6	21.5	26.7	16.5	20.9	16.6	66.1	65.7	16.9
25	16.3	15.3	15.2	16.0	15.3	16.5	17.2	17.5	17.3	17.0
26	15.7	16.8	16.7	18.7	16.5	15.9	20.7	17.7	17.4	17.1
27	13.9	25.8	25.8	23.7	25.9	14.5	18.5	25.1	26.1	24.1
28	26.7	68.8	28.3	69.6	24.9	25.5	31.3	178.6	176.6	25.0
29	28.5		29.1	23.6	177.9	70.5	25.1	28.6	33.2	182.5
30	21.4	103.6	16.9	33.2	20.3	25.6	31.9	25.2	23.8	21.1
OCH₃					51.7
1′					173.5			93.9	93.7
2′					34.6			78.6	78.6
3′					23.3			78.0	79.0
4′–11′					28.9–29.4			70.8	70.6
5′								78.8	79.2
6′								62.2	62.0
1″								103.4	104.6
2″								75.7	76.0
3″								77.8	78.4
4′’								72.5	72.7
5″								77.9	78.4
6″								63.7	63.8
12′					31.7
13′					NR
14′					13.9
Ref	[191]	[61]	[96]	[192]	[68]	[191]	[193]	[194]	[194]	[61]
C	O21	O22 ^a	O23	O24	O25	O26	O27	O28 ^a	O29	O30
1	79.6	40.0	39.5	34.7	33.4	34.1	39.1	212.9	40.3	38.7
2	44.5	34.4	34.3	29.4	25.4	22.7	27.3	45.4	23.9	23.8
3	172.4	215.9	218.1	98.0	75.8	78.0	78.7	79.0	80.2	81.2
4	56.0	47.8	47.6	40.0	37.5	36.7	39.2	40.1	38.3	37.1
5	85.0	55.1	55.3	50.2	48.4	49.7	55.0	54.9	55.2	56.0
6	33.2	19.0	19.9	19.4	17.4	17.7	17.5	18.1	17.7	18.2
7	27.6	32.1	32.8	30.8	32.6	32.5	32.9	34.4	34.0	35.1
8	43.2	45.3	40.0	38.5	43.5	43.5	46.3	40.7	44.1	40.3
9	55.2	61.2	46.9	41.6	61.6	61.6	60.4	42.8	54.2	50.5
10	44.5	37.0	36.9	35.0	37.1	37.0	37.4	53.5	39.3	37.1
11	67.3	198.9	23.9	23.6	200.3	200.1	195.3	24.4	75.3	24.8
12	133.5	128.4	124.7	122.3	128.3	128.2	142.8	26.7	202.2	124.2
13	139.8	170.6	140.5	143.4	169.4	169.3	138.3	39.6	83.2	144.1
14	42.6	43.7	42.9	41.6	45.6	45.6	41.5	43.7	44.8	42.1
15	19.8	26.7	25.4	25.8	25.7	25.8	26.5	27.8	22.9	27.2
16	34.1	26.9	24.5	28.0	22.0	21.5	26.7	31.3	39.1	27.5
17	51.4	32.5	35.5	36.0	37.0	37.0	31.3	32.5	33.5	32.0
18	37.8	47.3	43.7	47.0	42.7	42.7	38.7	140.7	49.1	47.4
19	40.5	40.8	40.0	46.5	44.9	45.0	41.3	132.6	38.3	46.9
20	47.7	36.0	39.7	36.0	31.0	31.0	30.9	32.5	31.5	31.1
21	215.9	29.9	39.7	73.8	33.9	33.8	34.7	33.4	34.5	34.8
22	40.4	36.4	83.3	45.0	30.6	30.6	36.9	31.1	30.0	37.2
23	21.0	21.5	27.0	27.0	28.4	28.0	28.0	28.6	28.2	28.0
24	20.3	26.5	21.7	18.0	22.3	21.9	15.5	16.6	16.4	16.6
25	13.8	15.9	15.2	67.7	16.3	16.3	16.5	16.1	16.4	15.5
26	19.1	18.5	16.7	17.0	18.6	18.6	18.7	17.0	20.9	16.5
27	22.6	23.4	25.3	25.1	23.6	23.5	23.2	15.1	18.9	25.7
28	26.8	28.7	24.2	28.1	69.7	69.7	29.2	63.6	31.4	28.7
29	28.4	28.2	182.7	16.6	32.9	32.9	33.1	31.4	32.3	33.2
30	21.3	65.3	21.2	28.8	23.4	23.4	23.4	29.7	24.5	23.7
OCH₃						21.7			21.4
C=O						170.7			171.2
1′									129.7	127.4
2′									130.1	115.4
3′									128.6	144.1
4′									133.2	146.6
5′									128.6	114.3
6′									130.1	122.2
7′									165.6	144.8
8′										116.0
9′										167.8
Ref	[117]	[190]	[195]	[196]	[154]	[154]	[54]	[190]	[197]	[198]
C	O31	O32	O33	O34	O36	O37	O38	O39	O40	O41
1	38.1	38.6	38.4	53.5	39.2	38.6	38.7	38.5	42.2	42.0
2	24.4	23.7	23.7	211.1	26.4	27.2	27.3	22.5	34.4	34.1
3	80.7	80.6	80.6	83.1	78.3	78.9	79.0	80.8	216.7	216.5
4	37.6	80.6	37.8	45.9	39.3	38.7	38.8	37.8	49.0	48.7
5	51.3	55.6	55.4	54.8	55.0	55.2	55.3	55.5	56.4	56.2
6	18.2	18.2	18.3	18.8	17.5	18.3	18.5	18.5	69.7	69.4
7	32.1	34.9	32.7	33.0	32.8	33.1	32.8	32.8	42.2	42.0
8	38.0	40.8	39.9	40.1	43.4	39.3	38.8	39.7	39.9	39.6
9	153.9	51.1	47.7	47.7	61.8	47.5	47.7	47.8	51.3	51.1
10	40.7	37.2	36.9	43.8	37.1	37.0	37.6	37.1	36.8	36.6
11	115.9	21.1	23.6	23.7	200.2	23.5	23.6	23.9	21.4	21.2
12	120.7	26.2	121.8	124.1	128.3	124.6	121.8	121.9	26.1	26.0
13	147.2	38.4	145.2	140.7	170.4	140.2	145.1	145.4	38.1	37.4
14	42.8	43.3	41.8	42.9	45.4	39.5	41.8	41.9	43.5	43.3
15	25.6	27.5	26.2	24.5	26.4	25.2	26.2	26.4	27.5	27.4
16	27.2	37.7	27.0	25.4	27.3	24.3	27.0	26.0	36.9	37.3
17	32.0	34.3	32.5	35.5	32.3	35.2	32.5	32.7	34.5	34.2
18	45.6	142.7	47.4	43.6	47.6	43.4	47.4	47.4	147.6	142.4
19	46.8	129.8	46.9	40.0	45.2	39.8	46.9	47.0	124.9	129.8
20	31.1	32.3	31.1	39.7	31.0	42.5	31.1	31.3	37.4	32.1
21	34.6	33.4	34.8	34.0	34.4	33.8	34.8	23.9	28.0	33.0
22	37.1	37.4	37.2	83.2	36.5	83.1	37.2	121.9	37.4	37.1
23	28.7	28.0	28.1	29.6	28.7	28.1	28.2	145.4	25.1	23.4
24	16.9	16.6	16.8	16.8	16.4	15.6	15.5	41.9	23.6	24.8
25	20.0	16.7	15.6	16.7	15.7	15.6	15.6	26.4	17.3	16.9
26	21.0	16.1	16.9	16.9	18.7	17.0	16.9	26.0	17.7	17.6
27	25.3	14.5	26.0	24.3	23.4	25.0	26.0	32.7	14.9	14.5
28	28.2	25.3	28.4	25.2	28.2	24.0	28.4	47.4	25.5	25.0
29	33.2	31.3	33.3	182.5	33.0	182.4	33.3	47.0	70.5	31.2
30	23.7	29.2	23.7	21.2	23.5	21.0	23.7	31.3	25.7	29.0
1′	127.8	173.7	173.5					173.9
2′	115.5	34.5	34.9					35.0
3′	143.8	25.2	25.2					25.4
4′	146.2	29.2	29.2					29.4–29.9
5′	114.3	29.3	29.3					29.4–29.9
6′	122.4	29.3	29.4					29.4–29.9
7′	144.4	29.7	29.6					29.4–29.9
8′	116.4	29.7	29.7					29.4–29.9
9′–13′	167.4	29.7	29.7					29.4–29.9
14′		29.7	29.7					31.2
15′		29.7	29.5					23.0
16′		31.9	31.9					14.4
17′		22.7	22.7
18′		14.1	14.1
Ref	[198]	[161]	[199]	[166]	[200]	[111]	[201]	[202]	[191]	[191]
C	O42	O43 ^c	O44	O45	O47 ^d	O50	O51 ^a	O52 ^c	O53	O54
1	38.9	42.5	40.6	128.4	40.1	39.3	47.8	34.6	41.5	40.1
2	34.0	35.3	34.8	143.9	35.0	34.2	68.6	42.2	175.2	37.4
3	216.9	217.0	218.6	201.2	219.0	217.9	83.8	76.6	180.3	213.6
4	47.1	48.6	48.4	44.0	48.0	47.5	39.8	37.2	46.0	44.8
5	52.4	56.8	55.9	53.9	56.0	55.3	55.9	48.5	48.9	53.6
6	30.3	20.9	20.1	18.8	20.3	19.7	18.9	37.9	20.7	23.9
7	72.9	32.2	31.5	32.7	26.7	32.1	33.2	18.1	32.1	31.6
8	43.3	44.3	44.4	40.5	40.5	39.8	48.2	32.8	39.3	39.1
9	46.9	55.4	50.7	43.1	47.5	46.8	48.2	43.2	39.4	45.3
10	36.7	38.9	38.1	38.4	37.8	36.7	38.6	55.6	41.6	36.7
11	23.5	68.3	76.6	23.6	24.0	23.7	23.5	67.1	23.9	22.0
12	122.5	128.7	122.8	123.0	123.4	123.3	122.5	126.1	124.6	122.5
13	143.8	147.2	148.9	143.4	143.5	143.2	144.9	147.7	140.1	143.8
14	45.3	43.0	42.2	41.9	43.4	41.9	42.2	41.4	43.3	41.8
15	29.2	27.3	26.5	25.7	26.3	25.4	28.3	25.1	24.4	27.6
16	22.3	28.0	27.2	28.1	29.0	22.2	23.7	26.5	25.3	23.0
17	36.7	33.1	32.3	37.4	39.5	36.9	46.7	31.5	35.4	46.5
18	43.0	49.0	48.1	43.9	49.8	41.1	41.7	47.0	43.6	41.3
19	46.4	43.3	42.6	39.9	44.2	39.9	42.0	30.9	39.8	45.8
20	31.0	44.8	43.3	42.5	46.0	42.4	31.0	43.5	39.6	30.7
21	34.1	34.2	33.3	36.2	40.6	28.5	34.3	30.9	33.9	33.8
22	30.8	39.5	38.6	75.8	78.7	29.8	33.3	38.0	83.2	32.4
23	26.4	27.4	27.0	27.3	26.6	21.6	29.4	28.4	28.5	116.0
24	21.5	22.2	21.9	21.9	21.7	26.6	16.9	22.1	23.4
25	15.0	17.0	16.7	20.0	15.5	15.3	17.5	16.4	19.2	13.1
26	9.7	18.9	18.4	17.5	17.2	16.7	17.7	17.8	17.2	17.0
27	25.9	26.3	25.5	25.4	26.2	25.4	26.2	26.5	23.7	25.8
28	69.6	29.3	29.0	19.9	25.8	69.0	180.2	28.4	25.2	180.4
29	33.1	29.3	29.3	184.0	34.3	184.5	33.3	28.0	182.4	33.0
30	23.8	178.9	183.3	23.8	181.0	19.2	23.8	179.2	20.7	23.5
OCH₃			54.1						52.2
Ref	[154]	[203]	[203]	[61]	[204]	[61]	[157]	[205]	[61]	[166]
C	O55	O56	O58 ^a	O60 ^a	O61	O62 ^a	O63 ^b	O65 ^b	O67 ^a	O68
1	36.8	39.6	33.6	38.9	33.6	37.9	38.2	38.9	38.9	38.5
2	32.4	34.4	26.2	28.1	26.2	25.1	26.6	28.2	27.6	26.7
3	217.7	217.8	75.2	78.0	70.8	81.9	79.7	79.6	73.7	78.7
4	39.1	47.7	37.8	39.7 *	47.4	55.4	38.0	40.1	42.9	38.6
5	55.3	55.6	49.1	55.8	49.1	46.9	48.0	56.5	48.8	55.1
6	19.5	20.0	18.6	18.8	19.7	20.3	19.5	19.0	18.7	18.2
7	33.8	32.5	32.9	33.2	32.7	32.6	33.7	33.4	33.6	32.5
8	39.3	40.1	40.3	37.3 *	39.8	39.9	39.6	41.2	39.8	39.7
9	47.4	47.1	47.7	48.1	46.7	47.1	49.6	48.9	48.2	47.5
10	46.9	37.0	37.3	37.9	37.6	37.9	39.9	37.8	37.3	36.8
11	23.6	24.0	23.8	23.8	23.5	23.5	20.2	24.4	23.8	23.4
12	122.4	123.0	123.2	122.7	121.7	120.9	124.3	123.5	122.7	123.1
13	143.6	144.3	144.4	144.7	145.1	143.0	144.7	144.5	145.0	143.2
14	41.7	42.1	42.0	42.2	41.9	42.0	43.2	43.5	42.2	41.5
15	32.2	27.3	25.9	28.3	26.0	35.9	24.7	26.5	28.4	25.2
16	21.4	26.3	23.0	24.0	26.9	73.1	27.9	29.0	23.8	21.8
17	46.6	32.7	37.6	46.6	32.5	48.6	41.2	39.5	46.7	36.7
18	41.0	46.4	41.7	41.6	47.3	41.2	56.6	49.9	42.0	41.1
19	45.8	40.5	41.4	42.0	46.7	47.5	40.0	44.3	46.5	40.1
20	30.7	42.8	42.8	35.9	31.1	30.9	43.9	46.2	31.0	42.1
21	32.4	29.2	29.5	29.6	34.7	35.8	76.0	40.7	34.3	28.4
22	26.4	36.1	30.8	32.9	37.1	32.8	41.5	78.8	33.3	29.7
23	27.7	26.8	29.2	28.4	183.2	206.4	28.7	28.3	68.2	27.9
24	15.0	21.7	22.7	16.5	24.2	10.2	17.4	16.1	13.1	15.4
25	15.0	15.5	15.7	15.3	13.1	15.4	16.1	15.7	16.0	15.3
26	17.0	17.0	17.0	17.4	16.7	17.2	16.3	17.3	17.5	16.5
27	25.8	26.1	26.0	26.2	25.9	27.1	26.7	26.3	26.2	25.7
28	183.9	28.4	68.3	180.2	28.4	174.8	21.0	25.8	180.4	68.6
29	33.0	185.1	181.5	28.2	33.3	33.2	182.3	34.1	33.3	181.7
30	23.5	19.4	20.1	65.5	23.7	24.5	25.2	181.1	23.8	19.1
Ref	[166]	[102]	[61]	[206]	[207]	[208]	[209]	[204]	[157]	[61]
C	O69 ^b	O70	O71 ^a	O72 ^a	O73	O75 ^a	O76	O77	O81	O82
1	42.0	38.1	213.0	38.5	38.5	49.6	38.3	78.7	34.9	32.5
2	28.0	23.4	45.4	28.0	27.4	170.6	23.5	172.2	25.2	26.0
3	80.0	81.0	78.4	78.1	78.7	182.0	80.8	110.9	76.0	76.1
4	39.7	37.7	40.0	39.5	38.7	45.4	37.9	36.4	37.4	37.3
5	57.1	55.4	54.7	55.3	55.2	55.2	55.2	48.8	48.7	47.3
6	68.7	18.2	18.2	18.8	18.3	20.7	18.3	17.6	18.3	18.3
7	41.6	32.6	33.2	32.9	32.6	33.4	32.6	34.5	33.0	32.5
8	40.7	39.4	39.7	41.1	39.3	41.1	39.8	41.1	43.6	37.0
9	49.4	47.6	39.7	54.8	47.6	45.9	47.5	41.0	56.4	48.9
10	37.6	37.0	52.7	37.1	37.0	38.5	36.8	40.1	38.2	33.0
11	24.5	23.4	25.7	126.0	23.1	74.5	23.7	22.1	67.6	23.4
12	124.0	122.6	123.2	127.0	122.1	121.4	121.6	24.2	126.1	122.6
13	144.4	143.6	144.1	136.6	143.4	149.8	145.2	133.5	148.0	143.7
14	43.3	41.6	42.5	42.5	41.6	43.1	41.7	45.2	41.8	41.7
15	28.8	27.7	28.3	33.3	27.7	25.8	26.1	26.4	26.0	26.0
16	24.1	22.9	23.7	25.6	23.4	27.5	26.9	39.3	28.0	32.5
17	47.9	46.6	46.8	48.7	46.6	32.9	32.5	34.6	34.7	25.2
18	41.9	41.0	42.3	133.8	41.3	47.2	47.2	133.9	45.8	35.0
19	41.4	45.7	46.2	41.0	45.8	41.6	46.7	38.7	46.7	46.6
20	36.8	30.7	31.0	32.8	30.6	36.1	31.1	33.3	36.3	50.0
21	29.3	33.6	34.3	37.5	33.8	30.0	34.7	35.4	73.9	74.0
22	33.1	32.5	33.2	36.3	32.3	36.6	37.1	36.4	45.1	36.3
23	28.4	28.1	29.0	28.5	28.1	28.2	28.1	19.3	28.3	45.4
24	17.6	17.2	16.8	16.0	15.6	23.3	16.8	24.3	22.3	28.2
25	17.3	15.2	15.0	18.4	15.3	17.7	15.6	15.0	16.7	22.3
26	18.8	16.7	18.1	17.1	16.8	17.1	16.9	18.1	18.1	16.8
27	26.5	25.9	26.0	20.1	26.0	25.5	26.0	21.3	26.3	15.2
28	181.8	184.0	180.1	178.9	181.0	28.4	28.4	23.8	28.5	26.0
29	74.4	33.1	33.3	32.4	33.1	28.2	33.3	32.3	28.9	28.3
30	19.5	23.6	23.8	24.4	23.6	65.6	23.7	24.0	16.9	29.0
1′							167.1
2′							116.2
3′							144.6
4′							127.1
5′							109.2
6′							146.8
7′							147.8
8′							114.6
9′							123.0
OCH₃		21.3					55.9
C=O		171.1
Ref	[210]	[211]	[157]	[212]	[27]	[190]	[213]	[214]	[187]	[187]
C	O84	O85	O86	O88	O89	O90	O91	O92	O93	O94
1	39.5	39.2	38.6	38.6	38.2	39.6	39.9	41.3	41.4	38.6
2	27.4	28.2	27.2	19.0	23.7	33.8	34.0	27.6	27.7	27.1
3	78.7	78.1	79.0	79.0	80.9	218.0	217.8	78.5	78.5	78.7
4	39.0	39.4	38.8	38.8	37.8	47.0	47.2	39.5	39.1	38.6
5	55.1	55.9	55.2	55.2	55.2	54.6	55.0	55.7	55.9	55.2
6	18.4	18.9	18.4	18.4	18.3	19.4	19.7	17.9	18.0	18.0
7	32.9	33.3	32.6	32.6	32.6	33.4	34.0	35.5	35.6	34.5
8	43.3	40.1	39.8	39.8	39.8	40.3	40.7	42.8	42.9	40.7
9	49.7	48.1	47.6	47.6	47.7	50.2	50.6	56.3	56.5	50.8
10	37.9	37.3	36.9	36.2	36.9	33.7	37.0	39.4	39.5	36.9
11	81.7	23.9	23.6	23.5	23.5	21.3	21.7	70.9	71.1	20.7
12	121.2	122.5	122.3	122.2	121.7	25.9	26.3	38.3	38.6	25.7
13	153.2	144.9	144.2	144.8	145.2	38.7	38.6	37.7	37.3	37.5
14	41.8	42.5	41.7	41.7	41.7	42.5	43.4	42.8	43.0	43.5
15	26.4	26.5	25.6	26.1	28.3	27.2	27.6	27.3	27.5	27.1
16	27.4	28.7	22.0	27.2	26.2	33.9	37.7	31.5	37.6	36.4
17	32.3	38.0	36.9	32.9	32.5	40.6	34.4	39.0	34.3	37.0
18	46.9	45.4	42.3	46.3	47.3	143.4	142.6	137.5	141.6	143.1
19	46.9	46.9	46.5	29.0	46.8	127.8	130.0	134.5	129.9	127.5
20	31.2	30.9	31.0	41.0	31.2	45.1	32.4	32.2	32.4	37.0
21	34.7	42.3	34.1	36.2	34.7	215.2	33.4	33.2	33.4	73.1
22	37.0	75.6	31.0	36.9	37.1	52.3	37.4	31.1	37.3	43.7
23	28.2	28.8	15.5	15.6	28.0	24.5	26.9	28.2	28.2	27.7
24	15.5	15.9	28.1	28.1	16.7	20.7	21.0	15.5	15.6	15.8
25	18.3	16.6	15.5	15.5	15.6	13.3	16.0	16.8	17.4	16.4
26	16.8	17.3	16.7	16.8	16.8	15.6	16.0	17.4	16.9	15.8
27	24.7	25.8	25.9	26.0	25.9	14.7	14.5	14.4	14.3	13.9
28	28.5	28.8	69.7	16.8	26.9	25.6	25.3	65.4	25.3	26.7
29	33.3	33.3	33.2	26.9	33.3	28.8	31.3	29.7	31.3	28.5
30	23.7	21.2	23.6	74.8	23.7	26.3	29.2	30.5	29.2	21.4
OCH₃					21.3
C=O					171.0
Ref	[215]	[216]	[217]	[218]	[219]	[191]	[220]	[191]	[220]	[191]
C	O95	O96	O97	O98	O99	O100	O101	O102
1	38.9	40.8	38.5	38.8	31.6	38.8	34.8	38.3
2	27.4	27.5	27.4	27.9	25.9	27.9	33.0	22.7
3	78.9	79.1	79.0	78.6	75.7	78.6	217.0	80.9
4	38.9	39.7	39.0	38.9	37.7	38.9	47.2	37.9
5	55.4	55.6	55.7	51.2	44.9	51.2	48.1	55.3
6	18.2	69.0	18.3	18.4	18.2	18.4	19.7	18.3
7	34.6	42.2	34.7	32.2	31.9	32.2	30.4	32.5
8	40.7	39.7	40.8	37.0	40.7	37.0	46.6	39.8
9	51.1	51.8	51.3	154.3	154.9	154.3	53.7	47.5
10	37.2	36.8	37.3	40.7	38.8	40.7	37.8	36.9
11	21.0	21.2	21.2	115.8	115.3	115.8	72.1	23.5
12	26.1	26.2	26.2	120.8	121.4	120.8	120.5	121.6
13	38.8	37.6	39.0	147.1	145.2	147.1	152.8	145.2
14	43.2	43.5	43.4	42.8	42.8	42.8	41.7	41.7
15	27.4	27.6	27.6	25.7	25.5	25.7	26.7	26.1
16	36.9	37.3	37.7	27.3	28.5	27.3	26.6	26.9
17	34.5	34.3	34.4	32.2	34.5	32.2	32.8	32.6
18	147.8	142.8	142.8	45.6	44.9	45.6	48.0	47.2
19	124.4	129.9	129.8	46.9	47.1	46.9	46.1	46.8
20	27.1	32.3	32.3	31.1	36.3	31.1	31.1	31.1
21	28.0	33.3	33.4	34.7	73.9	34.7	34.6	34.7
22	37.5	40.8	37.4	37.2	45.3	37.2	36.9	37.1
23	27.9	27.6	28.0	28.0	28.3	28.8	27.9	28.1
24	15.4	16.8	15.4	16.6	22.4	15.1	19.4	16.8
25	16.7	18.1	16.1	15.5	25.1	20.1	19.1	15.5
26	16.1	17.5	16.7	16.5	20.9	21.0	99.1	16.8
27	14.7	14.8	14.6	25.7	20.1	25.3	23.6	25.9
28	25.5	25.2	25.3	28.7	28.6	28.3	28.7	28.4
29	70.6	31.3	31.3	33.2	28.9	23.7	33.3	33.3
30	25.7	29.1	29.2	23.7	16.9	33.2	23.7	23.7
1′								127.3
2′								109.3
3′								147.0
4′								146.6
5′								114.8
6′								120.8
7′								76.4
8′								76.0
9′								62.9
OCH₃								56.0
1′								128.5
2′								116.6
3′								143.8
4′								144.8
5′								117.5
6′								122.2
7′								143.7
8′								117.3
9′								167.0
CH₃								20.7
C=O								170.4
Ref	[191]	[191]	[220]	[198]	[187]	[68]	[221]	[126]

Ref: References; * Values bearing the same superscript are interchangeable; NR: Not reported; Solvent: CDCl₃; ^a C₅D₅N; ^b CD₃OD; ^c CD₃COCD₃; ^d CD₃OD; ¹³C-NMR data of some compounds were not found. In these cases, the reported identification was performed by comparison of other physical data: O59 [222], O74 (m.p., IR, MS, ¹³C-NMR of acetylated compound) [102], O78 (m.p., MS, ¹H-NMR, UV, [α]_D) [223], O79 (m.p., MS, IR, UV, [α]_D) [224], O80, O83 and 087. ¹³C-NMR data of O35 [225], O46 [226], O48 [226], O49 [166], O57 [226], O64 [227], O66 [226] were reported, but the chemical shifts were not attributed to each carbon atom.