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. 2022 Jan 31;27(3):959. doi: 10.3390/molecules27030959

Table 8.

13C-NMR data of pentacyclic triterpenoids classified as others isolated from Celastraceae species (2001–2021).

C OT3 OT4 OT5 OT6 OT7 OT8 OT9 a OT10 a OT11 a OT12
1 39.6 38.9 104.6 18.2 37.8 37.2 104.5 106.2 121.3 36.6
2 34.2 27.5 144.7 27.8 27.1 194.7 147.5 146.9 182.0 34.8
3 218.2 78.4 144.2 76.3 79.0 200.1 144.2 144.4 182.2 217.1
4 47.4 39.0 118.0 40.8 38.7 123.8 118.1 128.7 131.4 47.6
5 54.9 55.3 129.8 141.6 55.5 154.8 129.8 117.6 142.1 53.2
6 19.7 18.5 122.5 122.0 18.8 75.0 122.6 121.6 121.3 26.3
7 33.7 33.4 127.9 23.5 41.3 122.9 127.9 130.0 153.2 22.6
8 41.6 41.7 131.3 47.8 38.9 154.0 131.3 141.7 47.6 41.0
9 49.6 50.4 135.6 34.8 49.2 51.6 135.3 132.2 144.8 147.4
10 36.8 37.2 129.5 49.6 38.0 71.6 129.5 131.8 158.2 39.3
11 21.6 21.1 25.5 34.6 17.5 28.2 29.3 129.0 128.3 115.6
12 23.9 24.0 32.8 30.5 37.7 29.5 35.9 138.1 38.9 36.1
13 49.6 49.5 102.5 37.7 36.0 38.2 54.5 44.1 41.6 36.7
14 42.1 42.1 43.6 39.5 158.0 40.3 156.8 49.0 43.2 38.2
15 32.6 33.7 38.8 32.5 116.9 28.5 34.1 31.3 24.8 29.6
16 21.6 21.7 40.2 35.7 33.6 35.6 41.4 38.8 38.6 35.8
17 54.9 54.9 42.6 30.5 37.6 30.7 41.6 32.4 33.2 42.8
18 44.7 44.8 46.0 41.9 48.0 43.4 50.4 43.2 48.2 52.0
19 41.9 41.9 32.8 39.3 31.1 30.6 36.8 32.7 32.6 20.1
20 27.3 27.4 40.2 33.1 33.8 41.7 41.9 41.9 41.7 28.2
21 46.4 46.5 36.8 29.5 28.1 29.9 30.8 31.0 31.1 59.6
22 148.6 148.6 36.9 27.9 35.3 35.9 35.5 36.2 34.5 30.7
23 26.6 28.2 11.6 28.9 28.0 9.5 11.6 11.6 11.2 22.0
24 21.1 15.7 25.4 15.5 25.5
25 15.7 16.7 20.5 16.1 15.4 27.0 20.7 19.5 27.7 21.6
26 16.4 15.9 23.2 18.1 25.9 21.5 28.0 20.1 20.5 16.9
27 16.6 16.7 23.2 20.4 21.1 28.7 108.3 23.4 20.5 15.3
28 16.1 16.1 25.1 32.0 29.9 31.7 31.3 31.7 31.8 13.9
29 110.1 110.2 180.5 74.4 73.9 178.8 184.7 183.6 183.2 22.1
30 25.0 25.0 26.3 26.0 24.6 32.5 25.9 32.5 34.0 23.0
Ref [94] [94] [139] [213] [213] [250] [139] [139] [139] [251]
C OT13 OT14 OT15 OT17 OT18 OT19 OT20 OT21
1 110.7 110.6 98.9 38.5 18.2 23.6 36.1 38.1
2 163.7 163.7 143.2 27.4 27.8 18.1 27.8 27.3
3 178.1 79.0 76.3 76.2 79.0 79.2
4 24.7 28.2 40.1 39.0 40.8 39.2 39.6 39.1
5 103.7 105.6 43.3 55.7 141.7 141.6 52.3 55.7
6 126.4 125.8 28.2 18.3 122.0 121.9 21.4 19.0
7 115.9 115.9 17.3 34.7 23.8 27.7 26.7 35.3
8 161.1 160.4 47.7 40.8 45.7 43.0 41.0 38.9
9 39.6 39.5 38.8 51.3 34.8 34.8 148.9 48.9
10 165.2 166.1 47.8 37.3 49.7 46.6 39.1 37.9
11 33.4 33.3 33.9 21.2 29.9 34.6 114.3 17.7
12 29.7 29.7 28.7 26.2 29.7 30.3 36.0 35.9
13 40.5 40.3 38.9 39.0 38.4 37.7 36.8 37.9
14 44.1 44.1 37.6 43.4 38.6 40.7 38.2 158.1
15 28.4 28.4 28.8 27.6 34.3 32.0 29.7 117.0
16 35.5 35.5 35.9 37.7 36.3 35.9 35.9 36.9
17 38.2 38.2 30.1 34.4 32.9 30.0 43.0 38.1
18 43.4 43.4 44.2 142.8 44.7 47.4 52.1 49.4
19 32.0 32.1 30.2 129.8 35.8 35.1 20.2 41.4
20 41.9 41.9 40.3 32.3 34.5 28.2 28.2 29.0
21 213.8 213.7 29.9 33.4 74.7 33.0 59.6 33.9
22 52.5 52.5 36.2 37.4 46.3 38.9 30.8 33.2
23 7.9 28.0 25.4 28.9 28.2 28.1
24 99.4 15.4 28.9 25.4 15.6 15.6
25 36.8 36.5 17.5 16.1 16.6 16.2 22.1 15.6
26 22.5 22.5 15.9 16.7 17.0 18.4 17.0 30.1
27 19.7 19.8 17.2 14.6 19.1 19.6 15.3 26.0
28 32.5 32.6 31.6 25.3 33.1 32.4 14.0 30.1
29 179.0 31.3 32.3 34.6 23.0 33.5
30 15.1 15.1 31.8 29.2 24.6 32.0 22.2 21.5
OCH3 50.5 51.0 51.3
Ref [252] [252] [196] [220] [196] [157] [253] [254]

Ref: References; NR: Not reported; Solvent CDCl3; a CD3OD; 13C-NMR data of some compounds were not found. In these cases, the reported identification was performed by comparison of other physical data: OT1 (m.p., [α]D, IR, 1H-NMR) [255], OT2 e OT16 (m.p., [α]D, IR, 1H-NMR, MS) [256].