Table 3.
Definitive screening design matrix and response for biodiesel yield.
Run | Experimental parameters of Transesterification |
Biodiesel Yield |
Error |
||||||
---|---|---|---|---|---|---|---|---|---|
(R-T)1 | (C-C)2 | (E-O-R)3 | (R-T)4 | (A-R)5 | (A-Y)6 | (P-Y)7 | Resid. | Std-Resd. | |
1 | 65 | 5 | 20 | 77 | 1000 | 92 | 91.91 | -0.005 | -0.04 |
2 | 65 | 2.75 | 15 | 61 | 875 | 92 | 92.03 | 0.174 | 1.27 |
3 | 65 | 0.5 | 10 | 45 | 750 | 92.4 | 92.15 | 0.025 | 0.23 |
4 | 80 | 0.5 | 15 | 77 | 1000 | 90.8 | 91.08 | 0.002 | 0.01 |
5 | 80 | 5 | 10 | 77 | 750 | 94.2 | 94.24 | -0.230 | -1.77 |
6 | 80 | 5 | 10 | 45 | 875 | 93.0 | 93.41 | 0.090 | 0.69 |
7 | 50 | 0.5 | 20 | 45 | 1000 | 89.66 | 89.64 | -0.015 | -0.14 |
8 | 50 | 5 | 15 | 45 | 750 | 92.8 | 92.97 | -0.038 | -0.30 |
9 | 50 | 0.5 | 20 | 77 | 875 | 89.2 | 89.23 | -0.167 | -1.28 |
10 | 80 | 0.5 | 20 | 45 | 750 | 90 | 90.09 | -0.005 | -0.04 |
11 | 65 | 2.75 | 15 | 61 | 875 | 92 | 92.03 | -0.120 | -1.11 |
12 | 50 | 5 | 20 | 61 | 750 | 91.8 | 91.63 | 0.131 | 1.20 |
13 | 80 | 0.5 | 10 | 61 | 1000 | 92.7 | 92.42 | -0.296 | -2.27 |
14 | 50 | 0.5 | 10 | 77 | 750 | 91.3 | 91.52 | 0.120 | 0.88 |
15 | 50 | 2.75 | 10 | 45 | 1000 | 93.2 | 93.15 | 0.027 | 0.21 |
16 | 80 | 5 | 20 | 45 | 1000 | 92.5 | 92.54 | 0.099 | 0.76 |
17 | 50 | 5 | 10 | 77 | 1000 | 94. | 93.97 | 0.052 | 0.38 |
18 | 80 | 2.75 | 20 | 77 | 750 | 91.04 | 90.91 | 0.157 | 1.15 |
Resid; Residual, Std-Resd; Standard residual.
Reaction time (min)
Catalyst concentration (w/w %)
Ethanol to oil ratio (g/g)
Reaction temperature (0C)
Agitation rate (rpm)
Actual yield (%)
Predicted yield (%)