Fig. 4. Solid-state structure of (tBuPBP)Pd{OC(O)CH3} with thermal ellipsoids at 30% probability. Hydrogen atoms are omitted for clarity. Selected distances (Å) and angles (°): Pd(1)–B(1) 1.975(2), Pd(1)–O(1) 2.1861(14), Pd(1)–P(1) 2.3256(5), Pd(1)–P(2) 2.3336(5), B(1)–Pd(1)–O(1) 174.99(7), B(1)–Pd(1)–P(1) 77.32(7), O(1)–Pd(1)–P(1) 100.17(4), B(1)–Pd(1)–P(2) 79.00(7), O(1)–Pd(1)–P(2) 103.05(4), P(1)–Pd(1)–P(2) 155.805(18).
