Table 1.
Summary of crystal data-collection statistics.
| KasQ–WT | KasQ–UDP | KasQ–UDP-Glc | |||||||
|---|---|---|---|---|---|---|---|---|---|
| PDB code | 7VYY | 7VZA | 7VZ6 | ||||||
| Wavelength (Å) | 1.0 | 1.0 | 1.0 | ||||||
| Space group | C2 | P1 | P1 | ||||||
| Cell dimensions | |||||||||
| a, b, c (Å) | 112.4 | 106.1 | 94.3 | 81.8 | 104.7 | 106.3 | 82.8 | 104.9 | 106.8 |
| α, β, γ (°) | 90 | 124.9 | 90 | 74.5 | 73.0 | 68.4 | 74.9 | 72.9 | 68.1 |
| Resolution (Å) | 25.45–2.44 (2.55–2.46) | 19.89–2.60 (2.68–2.60) | 21.56–2.10 (2.18–2.10) | ||||||
| R merge | 0.031 (0.387) | 0.023 (0.365) | 0.035 (0.296) | ||||||
| I/I | 26.6 (2.4) | 23.8 (1.9) | 19.7 (2.7) | ||||||
| Completeness (%) | 85.9 (86) | 93.9 (94.1) | 95.2 (95.1) | ||||||
| Redundancy | 3.6 (3.9) | 2.4 (2.5) | 2.2 (2.1) | ||||||
| Refinement | |||||||||
| Resolution (Å) | 25.45–2.44 (2.55–2.44) | 19.9–2.58 (2.68–2.58) | 21.5–2.09 (2.14–2.09) | ||||||
| No. reflections | 28,957 | 91,395 | 176,474 | ||||||
| Rwork/Rfree | 0.22/0.27 | 0.21/0.24 | 0.20/0.22 | ||||||
| R.m.s deviations | |||||||||
| Bond lengths (Å) | 0.66 | 0.66 | 0.70 | ||||||
| Bond angles (°) | 0.77 | 0.79 | 0.84 | ||||||