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. 2021 Jan 29;40(4):539–556. doi: 10.1021/acs.organomet.0c00787

Figure 9.

Figure 9

Thermal ellipsoid plot (50% probability) of the cation of 9f·Et2O along with the labeling scheme. The solvent molecule and the hydrogen atoms bonded to carbon have been omitted for clarity. Selected bond lengths (Å) and angles (deg): N(1)–C(8) = 1.5209(19), C(11)–C(12) = 1.522(2), C(11)–C(14) = 1.557(2), C(14)–O(4) = 1.4423(18), C(17)–O(3) = 1.2010(19), C(17)–O(4) = 1.3514(19), C(16)–C(17) = 1.499(2); C(1)–C(11)–C(12) = 107.19(12), C(11)–C(14)–O(4) = 109.88(12), C(14)–O(4)–C(17) = 111.86(11), O(4)–C(17)–C(16) = 111.77(13), C(17)–C(16)–C(15) = 104.53(12), C(16)–C(15)–C(14) = 104.02(12), C(15)–C(14)–O(4) = 106.07(11).