| Crystal data |
| Chemical formula |
[Ag(C9H16N3O2P)]BF4
|
|
M
r
|
423.90 |
| Crystal system, space group |
Monoclinic, C
c
|
| Temperature (K) |
293 |
|
a, b, c (Å) |
10.116 (5), 12.186 (5), 10.979 (5) |
| β (°) |
98.260 (5) |
|
V (Å3) |
1339.4 (11) |
|
Z
|
4 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
1.68 |
| Crystal size (mm) |
0.35 × 0.2 × 0.15 |
| |
| Data collection |
| Diffractometer |
Enraf–Nonius CAD-4 |
| Absorption correction |
ψ scan (North et al., 1968 ▸) |
|
T
min, T
max
|
0.558, 0.755 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
1358, 1313, 1299 |
|
R
int
|
0.009 |
| (sin θ/λ)max (Å−1) |
0.605 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.048, 0.123, 1.13 |
| No. of reflections |
1313 |
| No. of parameters |
190 |
| No. of restraints |
2 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
1.20, −1.54 |
| Absolute structure |
Classical Flack method preferred over Parsons because s.u. lower |
| Absolute structure parameter |
0.13 (6) |
