Bruker D8 QUEST CMOS PHOTON II diffractometer | 8352 independent reflections |
Radiation source: sealed x-ray tube, Mo | 6158 reflections with I > 2σ(I) |
Graphite monochromator | Rint = 0.077 |
Detector resolution: 7.39 pixels mm-1 | θmax = 26.2°, θmin = 2.9° |
ω and φ scans | h = −14→14 |
Absorption correction: multi-scan (SADABS; Bruker, 2016) | k = −14→14 |
Tmin = 0.684, Tmax = 0.745 | l = −22→22 |
78843 measured reflections |