| Refinement on F2 | Hydrogen site location: mixed |
| Least-squares matrix: full | H atoms treated by a mixture of independent and constrained refinement |
| R[F2 > 2σ(F2)] = 0.040 | w = 1/[σ2(Fo2) + (0.0432P)2 + 1.7899P] where P = (Fo2 + 2Fc2)/3 |
| wR(F2) = 0.103 | (Δ/σ)max = 0.001 |
| S = 1.09 | Δρmax = 0.82 e Å−3 |
| 8226 reflections | Δρmin = −0.69 e Å−3 |
| 545 parameters | Extinction correction: SHELXL2016/6 (Sheldrick 2015b), Fc*=kFc[1+0.001xFc2λ3/sin(2θ)]-1/4 |
| 10 restraints | Extinction coefficient: 0.00080 (10) |
| Primary atom site location: dual |