| Xcalibur, Ruby, Gemini diffractometer | 6698 reflections with I > 2σ(I) |
| Detector resolution: 10.5081 pixels mm-1 | Rint = 0.089 |
| ω scans | θmax = 76.0°, θmin = 3.1° |
| Absorption correction: analytical (CrysalisPro; Rigaku OD, 2015) | h = −18→13 |
| Tmin = 0.484, Tmax = 0.908 | k = −18→17 |
| 17610 measured reflections | l = −25→24 |
| 8591 independent reflections |
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