Refinement on F2	Primary atom site location: structure-invariant direct methods
Least-squares matrix: full	Secondary atom site location: difference Fourier map
R[F2 > 2σ(F2)] = 0.111	Hydrogen site location: mixed
wR(F2) = 0.277	H-atom parameters constrained
S = 1.06	w = 1/[σ2(Fo2) + (0.1511P)2 + 16.9004P] where P = (Fo2 + 2Fc2)/3
8591 reflections	(Δ/σ)max = 0.001
537 parameters	Δρmax = 4.24 e Å−3
78 restraints	Δρmin = −0.65 e Å−3