| Bruker D8 Venture/Photon 100 CMOS diffractometer | 3001 independent reflections |
| Radiation source: fine-focus sealed tube | 2585 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.045 |
| Detector resolution: 10.4167 pixels mm-1 | θmax = 27.5°, θmin = 2.6° |
| φ and ω scans | h = −11→11 |
| Absorption correction: multi-scan (SADABS; Krause et al., 2015) | k = −12→12 |
| Tmin = 0.690, Tmax = 0.746 | l = −20→20 |
| 56046 measured reflections |