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. 2022 Feb 3;78(Pt 3):275–281. doi: 10.1107/S2056989022000962
Bruker D8 Venture/Photon 100 CMOS diffractometer 3001 independent reflections
Radiation source: fine-focus sealed tube 2585 reflections with I > 2σ(I)
Graphite monochromator Rint = 0.045
Detector resolution: 10.4167 pixels mm-1 θmax = 27.5°, θmin = 2.6°
φ and ω scans h = −11→11
Absorption correction: multi-scan (SADABS; Krause et al., 2015) k = −12→12
Tmin = 0.690, Tmax = 0.746 l = −20→20
56046 measured reflections