Bruker D8 Venture/Photon 100 CMOS diffractometer | 3391 independent reflections |
Radiation source: fine-focus sealed tube | 2702 reflections with I > 2σ(I) |
Graphite monochromator | Rint = 0.054 |
Detector resolution: 10.4167 pixels mm-1 | θmax = 28.0°, θmin = 3.0° |
φ and ω scans | h = −17→17 |
Absorption correction: multi-scan (SADABS; Krause et al., 2015) | k = −17→17 |
Tmin = 0.390, Tmax = 0.746 | l = −10→10 |
54241 measured reflections |