| Crystal data |
| Chemical formula |
C42H48N6O18Tm2
|
|
M
r
|
1262.72 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
296 |
|
a, b, c (Å) |
8.9659 (6), 10.9722 (7), 12.8027 (8) |
| α, β, γ (°) |
88.195 (3), 71.599 (3), 74.402 (3) |
|
V (Å3) |
1149.10 (13) |
|
Z
|
1 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
3.92 |
| Crystal size (mm) |
0.32 × 0.18 × 0.16 |
| |
| Data collection |
| Diffractometer |
Bruker Kappa APEXII CCD |
| Absorption correction |
Multi-scan (SADABS; Krause et al., 2015 ▸) |
|
T
min, T
max
|
0.983, 0.986 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
13239, 4891, 4358 |
|
R
int
|
0.037 |
| (sin θ/λ)max (Å−1) |
0.639 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.029, 0.064, 1.04 |
| No. of reflections |
4891 |
| No. of parameters |
343 |
| No. of restraints |
19 |
| H-atom treatment |
H atoms treated by a mixture of independent and constrained refinement |
| Δρmax, Δρmin (e Å−3) |
1.80, −1.07 |
