Sb1—S4 | 2.3195 (13) | N12—H12 | 1.0000 |
Sb1—S1 | 2.3200 (12) | C13—C14 | 1.510 (8) |
Sb1—S3 | 2.3221 (12) | C13—H13A | 0.9900 |
Sb1—S2 | 2.3382 (11) | C13—H13B | 0.9900 |
S1—Co1 | 2.7258 (12) | C14—C15 | 1.514 (7) |
S2—Co2 | 2.6932 (11) | C14—H14A | 0.9900 |
S3—Co3 | 2.7821 (12) | C14—H14B | 0.9900 |
Co1—N2i | 1.990 (4) | C15—H15A | 0.9900 |
Co1—N2 | 1.990 (4) | C15—H15B | 0.9900 |
Co1—N1 | 1.993 (4) | Co3—N22 | 1.976 (4) |
Co1—N1i | 1.993 (4) | Co3—N22iii | 1.976 (4) |
N1—C1 | 1.468 (6) | Co3—N21 | 1.985 (4) |
N1—C5i | 1.470 (7) | Co3—N21iii | 1.985 (4) |
N1—H1 | 1.0000 | N21—C21 | 1.472 (7) |
C1—C2 | 1.504 (8) | N21—C25iii | 1.488 (6) |
C1—H1A | 0.9900 | N21—H21 | 1.0000 |
C1—H1B | 0.9900 | C21—C22 | 1.506 (8) |
C2—N2 | 1.481 (6) | C21—H21A | 0.9900 |
C2—H2A | 0.9900 | C21—H21B | 0.9900 |
C2—H2B | 0.9900 | C22—N22 | 1.486 (7) |
N2—C3 | 1.476 (6) | C22—H22A | 0.9900 |
N2—H2 | 1.0000 | C22—H22B | 0.9900 |
C3—C4 | 1.511 (8) | N22—C23 | 1.468 (6) |
C3—H3A | 0.9900 | N22—H22 | 1.0000 |
C3—H3B | 0.9900 | C23—C24 | 1.506 (9) |
C4—C5 | 1.517 (8) | C23—H23A | 0.9900 |
C4—H4A | 0.9900 | C23—H23B | 0.9900 |
C4—H4B | 0.9900 | C24—C25 | 1.510 (8) |
C5—H5A | 0.9900 | C24—H24A | 0.9900 |
C5—H5B | 0.9900 | C24—H24B | 0.9900 |
Co2—N11ii | 1.975 (4) | C25—H25A | 0.9900 |
Co2—N11 | 1.975 (4) | C25—H25B | 0.9900 |
Co2—N12 | 1.985 (4) | O1—H1C | 0.8400 |
Co2—N12ii | 1.985 (4) | O1—H1D | 0.8400 |
N11—C15ii | 1.475 (6) | N31—C31 | 1.145 (15) |
N11—C11 | 1.486 (6) | C31—C32 | 1.442 (17) |
N11—H11 | 1.0000 | C32—H32A | 0.9800 |
C11—C12 | 1.514 (7) | C32—H32B | 0.9800 |
C11—H11A | 0.9900 | C32—H32C | 0.9800 |
C11—H11B | 0.9900 | N31'—C31' | 1.145 (15) |
C12—N12 | 1.470 (6) | C31'—C32' | 1.442 (16) |
C12—H12A | 0.9900 | C32'—H32D | 0.9800 |
C12—H12B | 0.9900 | C32'—H32E | 0.9800 |
N12—C13 | 1.474 (6) | C32'—H32F | 0.9800 |
S4—Sb1—S1 | 109.86 (5) | H12A—C12—H12B | 108.4 |
S4—Sb1—S3 | 110.64 (5) | C12—N12—C13 | 111.3 (4) |
S1—Sb1—S3 | 110.81 (5) | C12—N12—Co2 | 108.0 (3) |
S4—Sb1—S2 | 110.32 (5) | C13—N12—Co2 | 119.6 (3) |
S1—Sb1—S2 | 105.36 (4) | C12—N12—H12 | 105.6 |
S3—Sb1—S2 | 109.73 (4) | C13—N12—H12 | 105.6 |
Sb1—S1—Co1 | 112.07 (5) | Co2—N12—H12 | 105.6 |
Sb1—S2—Co2 | 122.01 (4) | N12—C13—C14 | 112.7 (4) |
Sb1—S3—Co3 | 119.94 (5) | N12—C13—H13A | 109.0 |
N2i—Co1—N2 | 180.00 (19) | C14—C13—H13A | 109.0 |
N2i—Co1—N1 | 93.50 (17) | N12—C13—H13B | 109.0 |
N2—Co1—N1 | 86.50 (17) | C14—C13—H13B | 109.0 |
N2i—Co1—N1i | 86.50 (17) | H13A—C13—H13B | 107.8 |
N2—Co1—N1i | 93.50 (17) | C13—C14—C15 | 113.7 (4) |
N1—Co1—N1i | 180.0 | C13—C14—H14A | 108.8 |
N2i—Co1—S1 | 89.02 (12) | C15—C14—H14A | 108.8 |
N2—Co1—S1 | 90.98 (12) | C13—C14—H14B | 108.8 |
N1—Co1—S1 | 88.50 (12) | C15—C14—H14B | 108.8 |
N1i—Co1—S1 | 91.50 (12) | H14A—C14—H14B | 107.7 |
N2i—Co1—S1i | 90.98 (12) | N11ii—C15—C14 | 111.5 (4) |
N2—Co1—S1i | 89.02 (12) | N11ii—C15—H15A | 109.3 |
N1—Co1—S1i | 91.50 (12) | C14—C15—H15A | 109.3 |
N1i—Co1—S1i | 88.50 (12) | N11ii—C15—H15B | 109.3 |
S1—Co1—S1i | 180.0 | C14—C15—H15B | 109.3 |
C1—N1—C5i | 111.8 (4) | H15A—C15—H15B | 108.0 |
C1—N1—Co1 | 107.1 (3) | N22—Co3—N22iii | 180.00 (19) |
C5i—N1—Co1 | 119.1 (3) | N22—Co3—N21 | 86.93 (17) |
C1—N1—H1 | 106.0 | N22iii—Co3—N21 | 93.07 (17) |
C5i—N1—H1 | 106.0 | N22—Co3—N21iii | 93.07 (17) |
Co1—N1—H1 | 106.0 | N22iii—Co3—N21iii | 86.93 (17) |
N1—C1—C2 | 108.2 (4) | N21—Co3—N21iii | 180.0 |
N1—C1—H1A | 110.1 | N22—Co3—S3iii | 87.74 (11) |
C2—C1—H1A | 110.1 | N22iii—Co3—S3iii | 92.26 (11) |
N1—C1—H1B | 110.1 | N21—Co3—S3iii | 87.89 (12) |
C2—C1—H1B | 110.1 | N21iii—Co3—S3iii | 92.11 (12) |
H1A—C1—H1B | 108.4 | N22—Co3—S3 | 92.26 (11) |
N2—C2—C1 | 107.9 (4) | N22iii—Co3—S3 | 87.74 (11) |
N2—C2—H2A | 110.1 | N21—Co3—S3 | 92.11 (12) |
C1—C2—H2A | 110.1 | N21iii—Co3—S3 | 87.89 (12) |
N2—C2—H2B | 110.1 | S3iii—Co3—S3 | 180.00 (5) |
C1—C2—H2B | 110.1 | C21—N21—C25iii | 111.9 (4) |
H2A—C2—H2B | 108.4 | C21—N21—Co3 | 106.4 (3) |
C3—N2—C2 | 111.7 (4) | C25iii—N21—Co3 | 119.8 (3) |
C3—N2—Co1 | 118.9 (3) | C21—N21—H21 | 105.9 |
C2—N2—Co1 | 107.0 (3) | C25iii—N21—H21 | 105.9 |
C3—N2—H2 | 106.2 | Co3—N21—H21 | 105.9 |
C2—N2—H2 | 106.2 | N21—C21—C22 | 107.7 (4) |
Co1—N2—H2 | 106.2 | N21—C21—H21A | 110.2 |
N2—C3—C4 | 112.0 (4) | C22—C21—H21A | 110.2 |
N2—C3—H3A | 109.2 | N21—C21—H21B | 110.2 |
C4—C3—H3A | 109.2 | C22—C21—H21B | 110.2 |
N2—C3—H3B | 109.2 | H21A—C21—H21B | 108.5 |
C4—C3—H3B | 109.2 | N22—C22—C21 | 107.0 (4) |
H3A—C3—H3B | 107.9 | N22—C22—H22A | 110.3 |
C3—C4—C5 | 114.6 (4) | C21—C22—H22A | 110.3 |
C3—C4—H4A | 108.6 | N22—C22—H22B | 110.3 |
C5—C4—H4A | 108.6 | C21—C22—H22B | 110.3 |
C3—C4—H4B | 108.6 | H22A—C22—H22B | 108.6 |
C5—C4—H4B | 108.6 | C23—N22—C22 | 112.3 (4) |
H4A—C4—H4B | 107.6 | C23—N22—Co3 | 119.9 (3) |
N1i—C5—C4 | 112.6 (4) | C22—N22—Co3 | 106.9 (3) |
N1i—C5—H5A | 109.1 | C23—N22—H22 | 105.6 |
C4—C5—H5A | 109.1 | C22—N22—H22 | 105.6 |
N1i—C5—H5B | 109.1 | Co3—N22—H22 | 105.6 |
C4—C5—H5B | 109.1 | N22—C23—C24 | 112.5 (4) |
H5A—C5—H5B | 107.8 | N22—C23—H23A | 109.1 |
N11ii—Co2—N11 | 180.0 | C24—C23—H23A | 109.1 |
N11ii—Co2—N12 | 93.73 (16) | N22—C23—H23B | 109.1 |
N11—Co2—N12 | 86.27 (16) | C24—C23—H23B | 109.1 |
N11ii—Co2—N12ii | 86.27 (16) | H23A—C23—H23B | 107.8 |
N11—Co2—N12ii | 93.73 (16) | C23—C24—C25 | 113.8 (5) |
N12—Co2—N12ii | 180.0 | C23—C24—H24A | 108.8 |
N11ii—Co2—S2ii | 86.16 (11) | C25—C24—H24A | 108.8 |
N11—Co2—S2ii | 93.84 (11) | C23—C24—H24B | 108.8 |
N12—Co2—S2ii | 91.31 (11) | C25—C24—H24B | 108.8 |
N12ii—Co2—S2ii | 88.69 (11) | H24A—C24—H24B | 107.7 |
N11ii—Co2—S2 | 93.84 (11) | N21iii—C25—C24 | 111.6 (4) |
N11—Co2—S2 | 86.16 (11) | N21iii—C25—H25A | 109.3 |
N12—Co2—S2 | 88.69 (11) | C24—C25—H25A | 109.3 |
N12ii—Co2—S2 | 91.31 (11) | N21iii—C25—H25B | 109.3 |
S2ii—Co2—S2 | 180.0 | C24—C25—H25B | 109.3 |
C15ii—N11—C11 | 111.4 (4) | H25A—C25—H25B | 108.0 |
C15ii—N11—Co2 | 118.1 (3) | H1C—O1—H1D | 102.1 |
C11—N11—Co2 | 108.6 (3) | N31—C31—C32 | 172 (5) |
C15ii—N11—H11 | 106.0 | C31—C32—H32A | 109.4 |
C11—N11—H11 | 106.0 | C31—C32—H32B | 109.5 |
Co2—N11—H11 | 106.0 | H32A—C32—H32B | 109.5 |
N11—C11—C12 | 107.6 (4) | C31—C32—H32C | 109.5 |
N11—C11—H11A | 110.2 | H32A—C32—H32C | 109.5 |
C12—C11—H11A | 110.2 | H32B—C32—H32C | 109.5 |
N11—C11—H11B | 110.2 | N31'—C31'—C32' | 172 (5) |
C12—C11—H11B | 110.2 | C31'—C32'—H32D | 109.5 |
H11A—C11—H11B | 108.5 | C31'—C32'—H32E | 109.5 |
N12—C12—C11 | 108.2 (4) | H32D—C32'—H32E | 109.5 |
N12—C12—H12A | 110.1 | C31'—C32'—H32F | 109.4 |
C11—C12—H12A | 110.1 | H32D—C32'—H32F | 109.5 |
N12—C12—H12B | 110.1 | H32E—C32'—H32F | 109.5 |
C11—C12—H12B | 110.1 |