Stoe IPDS-2 diffractometer | 5078 reflections with I > 2σ(I) |
ω scans | Rint = 0.030 |
Absorption correction: numerical (X-Red and X-Shape; Stoe, 2008) | θmax = 27.0°, θmin = 1.6° |
Tmin = 0.649, Tmax = 0.774 | h = −11→11 |
15304 measured reflections | k = −16→16 |
6098 independent reflections | l = −17→17 |