Refinement on F2 | Hydrogen site location: mixed |
Least-squares matrix: full | H-atom parameters constrained |
R[F2 > 2σ(F2)] = 0.047 | w = 1/[σ2(Fo2) + (0.084P)2 + 0.1597P] where P = (Fo2 + 2Fc2)/3 |
wR(F2) = 0.126 | (Δ/σ)max = 0.047 |
S = 1.06 | Δρmax = 0.81 e Å−3 |
6098 reflections | Δρmin = −1.56 e Å−3 |
321 parameters | Extinction correction: SHELXL2016/6 (Sheldrick 2015b), Fc*=kFc[1+0.001xFc2λ3/sin(2θ)]-1/4 |
87 restraints | Extinction coefficient: 0.0136 (11) |