| Crystal data |
| Chemical formula |
[Co3(SbS4)2(C10H24N4)3]·2C2H3N·2H2O |
|
M
r
|
1395.90 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
200 |
|
a, b, c (Å) |
8.7292 (3), 12.9680 (5), 13.8936 (5) |
| α, β, γ (°) |
66.218 (3), 77.035 (3), 83.321 (3) |
|
V (Å3) |
1401.93 (9) |
|
Z
|
1 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
2.16 |
| Crystal size (mm) |
0.15 × 0.10 × 0.07 |
| |
| Data collection |
| Diffractometer |
Stoe IPDS2 |
| Absorption correction |
Numerical (X-RED and X-SHAPE; Stoe, 2008 ▸) |
|
T
min, T
max
|
0.649, 0.774 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
15304, 6098, 5078 |
|
R
int
|
0.030 |
| (sin θ/λ)max (Å−1) |
0.639 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.047, 0.126, 1.06 |
| No. of reflections |
6098 |
| No. of parameters |
321 |
| No. of restraints |
87 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
0.81, −1.56 |
