Table 3. Data collection and processing.
Values in parentheses are for the outer shell.
| PaGT3 + UDP-2FGlc | PaGT3 + kaempferol + UDP-2FGlc | PaGT3 + capsaicin + UDP-2FGlc | |
|---|---|---|---|
| X-ray source | BL44XU, SPring-8 | BL44XU, SPring-8 | BL44XU, SPring-8 |
| Detector | EIGER X 16M | EIGER X 16M | EIGER X 16M |
| Wavelength (Å) | 0.9 | 0.9 | 0.9 |
| Space group | P212121 | P212121 | P212121 |
| a, b, c (Å) | 94.2, 103.8, 110.0 | 93.8, 103.1, 108.8 | 94.2, 103.0, 109.6 |
| Resolution range (Å) | 50.00–2.20 (2.26–2.20) | 50.00–1.85 (1.91–1.85) | 50.00–2.60 (2.71–2.60) |
| Total No. of reflections | 369985 | 600931 | 225962 |
| No. of unique reflections | 55339 (5439) | 89096 (8762) | 33386 (3286) |
| R merge (%) | 5.1 (65.8) | 5.3 (44.6) | 7.3 (59.9) |
| R meas (%) | 5.5 (71.3) | 5.8 (48.2) | 7.9 (64.7) |
| 〈I/σ(I)〉 | 21.10 (2.96) | 19.70 (3.46) | 17.86 (3.12) |
| CC1/2 | (0.85) | (0.92) | (0.89) |
| Completeness (%) | 99.9 (100) | 98.2 (97.8) | 99.5 (99.3) |
| Multiplicity | 6.7 (6.8) | 6.7 (7.0) | 6.8 (7.1) |