Table 1.
Entry | Catalyst/co-Catalyst | Conditions | PFPy Yield (%) |
---|---|---|---|
1 | Fe | 500 °C | 40–43 |
2 | Zn | THF, 80 °C, 5 h | 18 |
3 | Zn/SOCl2 | Sulfolane, 80 °C, 5 h | 30 |
4 | Zn/CuSO4 | Sulfolane, 80 °C, 5 h | 38 |
5 | Zn/CuSO4 | Diglyme, 80 °C, 5 h | 29 |
6 | Zn/complex NiCl2x6H2O + bpy | DMA, 80 °C, 5 h | 34 |