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. 2022 Mar 3;27(5):1672. doi: 10.3390/molecules27051672

Table 3.

Analytical procedures of sulfur volatile compounds in whisky.

Sample Preparation Separation Detector References
headspace GC FPD Ronkaine et al. [30]
headspace GC FPD Leppänen et al. [66]
liquid/liquid extraction GC MS Masuda and Nishimura [31]
liquid/liquid extraction MDGC MS, ECD Carter-Tijmstra [34]
not shown MDGC SCD, NTD, MS MacNamara an Hoffmann [38]
vacuum distillation, preparative GC MDGC SCD, MS MacNamara [35]
counter-current chromatography GC MS Taniguchi et al. [33]
headspace SPME GC MS Campillo et al. [32]
headspace Tenax GC SCD Harrison et al. [14]
full evaporation dynamic headspace MDGC SCD, NCD, MS Ochiai et al. [36]
headspace SPME GC MS Dziekońska-Kubczak et al. [67]
solvent assisted flavor extraction GC MS Kerley and Munafo [68]
headspace SPME GC MS Daute et al. [13]