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. 2022 Mar 17;14(3):218. doi: 10.3390/toxins14030218

Table 2.

Recovery percentages (% ± SD) for atropine (At) and scopolamine (Sc) in standard solutions using HMS and SBA-15 functionalized mesostructured silicas as dSPE or SPE sorbents.

Standard
Solution
(µg/mL)
Sorbent
Amount (mg)
SBA-15-SO3 HMS-SO3
dSPE a SPE b dSPE a SPE b
At c Sc d At c Sc d At c Sc d At c Sc d
0.01 150 77 ± 7 85 ± 3 92 ± 1 118 ± 1 102 ± 11 101 ± 11 95 ± 6 99 ± 7
100 72 ± 1 70 ± 2 95 ± 1 116 ± 2 79 ± 4 74 ± 8 80 ± 3 99 ± 8
0.001 100 85 ± 2 70 ± 2 97 ± 1 91 ± 2 83 ± 9 82 ± 8 93 ± 2 104 ± 5

a dSPE: dispersive solid phase extraction; for experimental conditions see Figure 3. b SPE: solid phase extraction; for experimental conditions see section Figure 3. c At: atropine, recovery ± SD (%). d Sc: scopolamine, recovery ± SD (%).