Table 2.
12 | |||
---|---|---|---|
Position | δ C a | δ H b | HMBC |
1 | 12.14 (1H, s) | ||
2 | 130.0, CH | 8.34 (1H, s) | 3, 3a, 7a |
3 | 114.7, C | ||
3a | 116.3, C | ||
4 | 148.7, C | ||
4-OH | 15.07 (1H, s) | 3a, 4, 5 | |
5 | 99.1, C | ||
6 | 128.6, CH | 7.42 (1H, s) | 4, 5, 7, 7a |
7 | 93.0, C | ||
7a | 136.1, C | ||
1′ | - | - | - |
2′ | 161.4, C | ||
2′-NH2 | 6.91 (2H, brs) | ||
3′ | - | - | - |
4′ | 159.3, C | ||
5′ | 104.6, CH | 7.23 (1H, d, 5) | 3, 4′, 6′ |
6′ | 159.4, CH | 8.17 (1H, d, 5) | 4′, 5′ |
a 125 MHz, multiplicity from HSQC; b 500 MHz (integration, multiplicity, J (Hz)).