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. 2022 Mar 17;14(6):1211. doi: 10.3390/polym14061211

Table 2.

Textural properties of aerogel-based scaffolds obtained from aqueous 6 wt.% alginate inks with different HA concentrations (0, 8, 16, 24 wt.%) and crosslinked by different strategies: CaCl2 0.5M1h/1M1h (aged aerogels), CaCl2 1 M (non-aged aerogels) and GA (GA-crosslinked aerogels). Notation: ABET: specific BET surface area, dp: BJH-mean pore diameter, Vp: BJH-specific pore volume.

Aerogel Scaffold ABET (m2/g) dp (nm) Vp (cm3/g) ρenv (g/cm3) ρskel (g/cm3) ε (%)
Alg 6%, HA 0%, CaCl2 1 M * 183 ± 9 19 ± 1 1.16 ± 0.06 0.14 ± 0.01 ǂ 1.18 ± 0.16 86.58 ± 2.26
Alg 6%, HA 8%, CaCl2 1 M * 118 ± 6 24 ± 1 0.99 ± 0.05 0.24 ± 0.03 ǂ 1.72 ± 0.09 85.25 ± 4.02
Alg 6%, HA 16%, CaCl2 1 M * 67 ± 3 26 ± 1 0.60 ± 0.03 0.29 ± 0.04 ǂ 1.93 ± 0.04 79.78 ± 3.92
Alg 6%, HA 24%, CaCl2 1 M * 29 ± 2 31 ± 2 0.21 ± 0.01 0.34 ±0.02 ǂ 1.72 ± 0.14 76.68 ± 3.54
Alg 6%, HA 0%, CaCl2 0.5M1h 453 ± 23 25 ± 1 3.21 ± 0.16 0.18 ± 0.01 ǂ 1.81 ± 0.08 90.32 ± 0.81
Alg 6%, HA 0%, CaCl2 1M1h 244 ± 12 24 ± 1 1.74 ± 0.1 0.19 ± 0.003 1.44 ± 0.09 86.78 ± 0.88
Alg 6%, HA 8%, CaCl2 1M1h 81 ± 4 26 ± 1 0.68 ± 0.03 0.41 ± 0.003 2.29 ± 0.03 82.27 ± 0.24
Alg 6%, HA 16%, CaCl2 1M1h 49 ± 3 28 ± 1 0.39 ± 0.02 0.55 ± 0.003 2.38 ± 0.04 76.86 ± 0.35
Alg 6%, HA 24%, CaCl2 1M1h 65 ± 3 28 ± 1 0.69 ± 0.03 0.63 ± 0.003 2.71 ± 0.05 76.77 ± 0.47
Alg 6%, CaCl2 1 M, GA 112 ± 6 19 ± 1 0.72 ± 0.04 0.22 ± 0.07 ǂ 1.49 ± 0.05 85.45 ± 4.60
Alg 6%, HA 8%, CaCl2 1 M, GA 91 ± 5 21 ± 1 0.66 ± 0.03 0.41 ± 0.09 ǂ 1.84 ± 0.04 77.50 ± 4.80
Alg 6%, HA 0%, CaCl2 1M1h, GA 26 ± 1 19 ± 1 0.15 ± 0.01 0.52 ± 0.09 1.96 ± 0.19 73.32 ± 2.62
Alg 6%, HA 8%, CaCl2 1M1h, GA 28 ± 1 24 ± 1 0.21 ± 0.01 0.68 ± 0.09 2.16 ± 0.09 68.58 ± 1.41
Alg 6%, HA 16%, CaCl2 1M1h, GA 21 ± 1 32 ± 2 0.24 ± 0.01 0.94 ± 0.20 2.33 ± 0.09 59.58 ± 1.47
Alg 6%, HA 24%, CaCl2 1M1h, GA 21 ± 1 24 ± 1 0.19 ±0.01 0.97 ± 0.13 2.37 ± 0.05 59.14 ± 0.87

* Data obtained from the literature (ref. [7]).ǂ Data calculated following the procedure reported in ref. [7]).