Table 1. Data collection and refinement statistics of human AMDHD2.
| AMDHD2+Zn+GlcN6P | AMDHD2+Zn | |
|---|---|---|
| Wavelength (Å) | 1.00 | 1.00 |
| Resolution range (Å) | 45.71–1.90(1.97–1.90) | 48.21–1.84(1.90–1.84) |
| Space group | P 212121 | P 212121 |
| a, b, c (Å) | 63.3, 161.4, 86.6 | 61.8, 84.3, 154.2 |
| α, β, γ (°) | 90, 90, 90 | 90, 90, 90 |
| Total reflections | 428,727 (42,693) | 468,961 (46,539) |
| Unique reflections | 70,760 (6907) | 71,036 (6953) |
| Multiplicity | 6.1 (6.2) | 6.6 (6.7) |
| Completeness (%) | 99.7 (98.3) | 99.9 (99.2) |
| Mean I/sigma(I) | 11.46 (1.16) | 12.53 (1.06) |
| Wilson B-factor | 34.7 | 29.7 |
| Rmerge (%) | 9.5 (140.4) | 10.2 (150.6) |
| Rmeas (%) | 10.4 (153.3) | 11.0 (163.3) |
| Rpim (%) | 4.2 (60.9) | 4.3 (62.5) |
| CC1/2 (%) | 99.9 (49.4) | 99.9 (49.9) |
| CC* (%) | 100 (81.3) | 100 (81.6) |
| Reflections used in refinement | 70,751 (6906) | 71,024 (6952) |
| Reflections used for R-free | 1980 (194) | 1992 (195) |
| Rwork (%) | 18.5 (31.7) | 18.2 (31.2) |
| Rfree (%) | 21.3 (29.6) | 20.6 (33.6) |
| CCwork (%) | 96.6 (73.4) | 96.6 (75.7) |
| CCfree (%) | 94.4 (73.1) | 95.4 (72.8) |
| Number of non-hydrogen atoms | 6361 | 6331 |
| Macromolecules | 5997 | 5999 |
| Ligands | 34 | 14 |
| Solvent | 330 | 318 |
| Protein residues | 801 | 798 |
| RMS (bonds) (Å) | 0.005 | 0.004 |
| RMS (angles) (°) | 0.69 | 0.70 |
| Ramachandran favored (%) | 96.9 | 97.1 |
| Ramachandran allowed (%) | 2.9 | 2.7 |
| Ramachandran outliers (%) | 0.25 | 0.25 |
| Rotamer outliers (%) | 0.32 | 0.32 |
| Clashscore | 0.67 | 0.92 |
| Average B-factor | 43.59 | 37.67 |
| Macromolecules | 43.81 | 37.76 |
| Ligands | 40.19 | 41.98 |
| Solvent | 40.10 | 35.72 |
| Number of TLS groups | 4 | 4 |
| PDB ID | 7NUT | 7NUU |
Statistics for the highest-resolution shell are shown in parentheses.