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. 2022 Apr 1;12(17):10219–10236. doi: 10.1039/d2ra00212d

Screening the reaction parameters for the synthesis of 6d.

graphic file with name d2ra00212d-u1.jpg
Entry Fe3−xBixO4/SiO2@l-ArgEt3+I/Zn(ii) (g)/solvent (3 mL)/temperature (°C) Time (h) Yield (%)
1 0.032/—/rt 24 32
2 0.032/—/60 12 20
3 0.032/H2O/rt 16 10
4 0.032/EtOH/rt 16 62
5 0.04/EtOH/rt 12 51
6 0.02/EtOH/rt 16 67
7 0.024/EtOH/rt 20 67
8 0.012/EtOH/rt 9 83
9 0.012/EtOH–H2O (1 : 1)/rt 12 10
10 0.012/EtOH–H2O (1 : 1)/50 10 40
11 0.012/PEG (2000)/rt 10 5
12 0.012/EtOH/0 20