Comparison of the synthesis of 6d with the previously reported procedure.
Entry | Conditions | Time/yield (%) | Ref. |
---|---|---|---|
1 | CH2Cl2/rt | 24 h/48 | 60 |
2 | Fe3−xBixO4/SiO2@l-ArgEt3+I−/Zn(ii) (0.012 g)/EtOH (3 mL)/rt | 9 h/83 | This work |
3 | Fe3−xBixO4/SiO2@l-ArgEt3+I−/Zn(ii) (0.012 g)/EtOH (3 mL)/rt/Us | 60 min/71 | This work |