Crystal plane index, corresponding 2θ, and the crystal system of products synthesized at various crystallization times.
| Time (h) | 0.5 | 1 | 2 | 3 | 4 |
|---|---|---|---|---|---|
| (111) | — | — | 6.0750 | 6.0780 | 6.0957 |
| (220) | — | — | 9.9855 | 9.9493 | 9.9610 |
| (311) | — | — | — | 11.6720 | 11.6918 |
| (331) | — | — | 15.3543 | 15.3798 | 15.3967 |
| (440) | — | — | 19.9835 | 20.0101 | 20.0242 |
| (533) | — | — | 23.2126 | 23.2429 | 23.2621 |
| (642) | — | — | 26.5670 | 26.5918 | 26.6048 |
| (751) | — | — | 30.8612 | 30.8770 | 30.8973 |
| Crystal system | — | — | Cubic | Cubic | Cubic |