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. 2022 Jan 26;12(6):3313–3321. doi: 10.1039/d1ra07798h

Crystal plane index, corresponding 2θ, and the crystal system of products synthesized at various crystallization times.

Time (h) 0.5 1 2 3 4
(111) 6.0750 6.0780 6.0957
(220) 9.9855 9.9493 9.9610
(311) 11.6720 11.6918
(331) 15.3543 15.3798 15.3967
(440) 19.9835 20.0101 20.0242
(533) 23.2126 23.2429 23.2621
(642) 26.5670 26.5918 26.6048
(751) 30.8612 30.8770 30.8973
Crystal system Cubic Cubic Cubic