Table 2.
Data collection and refinement statistics (molecular replacement).
| Crystal Data | |
|---|---|
| Data collection | CiIFNa |
| Space group | C121 |
| Cell dimensions | |
| a, b, c (Å) | 84.617, 32.767, 56.762 |
| α, β, γ (°) | 90, 102.21, 90 |
| Resolution (Å) | 27.75–1.58 |
| Wavelength | 0.97923 Å |
| Beamline | BL18U1 |
| Refinement | |
| Resolution (Å) | 35.3–1.35 |
| No. reflections | 1113 |
| Rwork/Rfree | 0.1799/0.2251 |
| No. atoms | 919 |
| Protein | 100 |
| Ligand/ion | |
| Water | 125 |
| B-factors | 17.0 |
| R.m.s. deviations | |
| Bond lengths (Å) | 0.012 |
| Bond angles (°) | 1.718 |
| Ramachandran statistics | |
| Preferred regions (%) | 100 |
| Allowed regions (%) Outlier (0.00%) |
0.00 0.00 |
Values in parentheses are for highest-resolution shell.