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. 2022 Feb 1;12(7):3990–3995. doi: 10.1039/d1ra06558k

Effect of catalyst amount and solvent on sulphoxidation of thioanisolea.

Entry Catalyst (mol%) TFE/water Yieldb (%)
1 0 2 : 1 Trace
2 5 2 : 1 40
3 10 2 : 1 70
4 20 2 : 1 68
5 10 1 : 0 9
6 10 1 : 2 49
7 10 0 : 1 0.15
a

Conditions: substrate (0.194 mmol), AA (1 eq.).

b

Yield determined by HPLC.