Substrate scope for electrochemical synthesis of quinazolinone derivativesa,b.
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Reaction conditions: undivided cell, Pt anode (1.0 cm × 1.0 cm), Pt cathode (1.0 cm × 1.0 cm), 1a (0.5 mmol), 2a (0.8 mmol), 4-oxo-TEMPO (0.1 mmol), TBAPF6 (0.15 M), CH3CN/H2O (v/v = 1 : 2, 3 mL), constant current 80 mA, under air at room temperature for 3 h.
Isolated yield.