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| Entries | Temperature (°C) | Yield (%) | M w | M z | Đ |
|---|---|---|---|---|---|
| 1 | r.t. | 70 | 7600 | 10 700 | 1.41 |
| 2 | 60 | 84 | 16 400 | 29 700 | 1.81 |
| 3 | 100 | 85 | 16 600 | 30 800 | 1.86 |
Carried out in DMF for 24 h, concentration: [1] = 0.213 M. [1] : [2] : [3] = 2 : 2 : 1.
