| Refinement on F2 | Hydrogen site location: inferred from neighbouring sites |
| R[F2 > 2σ(F2)] = 0.049 | H atoms treated by a mixture of independent and constrained refinement |
| wR(F2) = 0.127 | w = 1/[σ2(Fo2) + (0.0686P)2 + 0.3253P] where P = (Fo2 + 2Fc2)/3 |
| S = 1.05 | (Δ/σ)max = 0.001 |
| 2907 reflections | Δρmax = 0.39 e Å−3 |
| 178 parameters | Δρmin = −0.29 e Å−3 |
| 0 restraints | Extinction correction: SHELXL |
| Primary atom site location: structure-invariant direct methods | Extinction coefficient: 0.259 (14) |
| Secondary atom site location: difference Fourier map |