Table 3. Experimental details.
| Crystal data | |
| Chemical formula | [Ag2V2F4O4(C9H9N3)4] |
| M r | 1094.39 |
| Crystal system, space group | Monoclinic, P21/c |
| Temperature (K) | 296 |
| a, b, c (Å) | 7.5484 (2), 21.2439 (6), 12.5910 (4) |
| β (°) | 90.910 (2) |
| V (Å3) | 2018.81 (10) |
| Z | 2 |
| Radiation type | Mo Kα |
| μ (mm−1) | 1.48 |
| Crystal size (mm) | 0.27 × 0.14 × 0.12 |
| Data collection | |
| Diffractometer | Bruker APEXII area-detector |
| Absorption correction | multi-scan (SADABS; Bruker, 2008 ▸) |
| T min, T max | 0.657, 0.856 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 22923, 5125, 3468 |
| R int | 0.044 |
| (sin θ/λ)max (Å−1) | 0.676 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.038, 0.078, 1.02 |
| No. of reflections | 5125 |
| No. of parameters | 323 |
| No. of restraints | 65 |
| H-atom treatment | H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) | 0.58, −0.42 |