| Tb1—O1 | 2.3632 (15) | N2—H2 | 0.849 (17) |
| Tb1—O2 | 2.3690 (15) | N2—C1 | 1.316 (3) |
| Tb1—O3 | 2.3525 (14) | N3—H3A | 0.865 (17) |
| Tb1—O4 | 2.4779 (19) | N3—H3B | 0.850 (17) |
| Tb1—O5 | 2.4959 (17) | N3—N4 | 1.414 (3) |
| Tb1—O7 | 2.4220 (15) | N4—H4 | 0.867 (17) |
| Tb1—N1 | 2.587 (2) | N4—C3 | 1.313 (3) |
| Tb1—N3 | 2.5640 (19) | N5—H5A | 0.857 (17) |
| Tb1—N5 | 2.5532 (18) | N5—H5B | 0.851 (17) |
| O1—C1 | 1.240 (2) | N5—N6 | 1.417 (3) |
| O2—C3 | 1.240 (2) | N6—H6 | 0.845 (17) |
| O3—C5 | 1.254 (2) | N6—C5 | 1.314 (3) |
| O4—N7 | 1.261 (3) | C1—C2 | 1.491 (3) |
| O5—N7 | 1.262 (3) | C2—H2A | 0.9600 |
| O6—N7 | 1.222 (3) | C2—H2B | 0.9600 |
| O7—N8 | 1.294 (2) | C2—H2C | 0.9600 |
| O8—N8 | 1.232 (2) | C3—C4 | 1.494 (3) |
| O9—N8 | 1.230 (2) | C4—H4A | 0.9600 |
| O10—N9 | 1.244 (2) | C4—H4B | 0.9600 |
| O11—N9 | 1.231 (3) | C4—H4C | 0.9600 |
| O12—N9 | 1.257 (2) | C5—C6 | 1.494 (3) |
| N1—H1A | 0.844 (17) | C6—H6A | 0.9600 |
| N1—H1B | 0.845 (17) | C6—H6B | 0.9600 |
| N1—N2 | 1.411 (3) | C6—H6C | 0.9600 |
| O1—Tb1—O2 | 69.15 (6) | H3A—N3—H3B | 106 (3) |
| O1—Tb1—O4 | 137.09 (7) | N4—N3—Tb1 | 111.81 (13) |
| O1—Tb1—O5 | 140.08 (6) | N4—N3—H3A | 108.2 (18) |
| O1—Tb1—O7 | 135.12 (5) | N4—N3—H3B | 109 (2) |
| O1—Tb1—N1 | 63.66 (6) | N3—N4—H4 | 120 (2) |
| O1—Tb1—N3 | 98.35 (6) | C3—N4—N3 | 118.22 (18) |
| O1—Tb1—N5 | 69.45 (6) | C3—N4—H4 | 121 (2) |
| O2—Tb1—O4 | 70.66 (7) | Tb1—N5—H5A | 118.0 (19) |
| O2—Tb1—O5 | 113.77 (6) | Tb1—N5—H5B | 106.4 (19) |
| O2—Tb1—O7 | 138.48 (5) | H5A—N5—H5B | 110 (3) |
| O2—Tb1—N1 | 114.19 (6) | N6—N5—Tb1 | 109.48 (12) |
| O2—Tb1—N3 | 64.41 (6) | N6—N5—H5A | 107.6 (19) |
| O2—Tb1—N5 | 76.73 (5) | N6—N5—H5B | 104.8 (19) |
| O3—Tb1—O1 | 79.00 (6) | N5—N6—H6 | 118.1 (18) |
| O3—Tb1—O2 | 137.59 (5) | C5—N6—N5 | 119.68 (17) |
| O3—Tb1—O4 | 124.67 (6) | C5—N6—H6 | 122.1 (18) |
| O3—Tb1—O5 | 74.51 (6) | O4—N7—O5 | 115.89 (19) |
| O3—Tb1—O7 | 83.93 (5) | O6—N7—O4 | 121.8 (3) |
| O3—Tb1—N1 | 72.54 (6) | O6—N7—O5 | 122.3 (3) |
| O3—Tb1—N3 | 150.36 (6) | O8—N8—O7 | 119.45 (18) |
| O3—Tb1—N5 | 66.06 (5) | O9—N8—O7 | 117.96 (19) |
| O4—Tb1—O5 | 50.93 (7) | O9—N8—O8 | 122.57 (19) |
| O4—Tb1—N1 | 150.97 (7) | O10—N9—O12 | 120.03 (19) |
| O4—Tb1—N3 | 77.11 (7) | O11—N9—O10 | 119.8 (2) |
| O4—Tb1—N5 | 87.34 (7) | O11—N9—O12 | 120.1 (2) |
| O5—Tb1—N1 | 131.95 (7) | O1—C1—N2 | 121.1 (2) |
| O5—Tb1—N3 | 119.27 (7) | O1—C1—C2 | 120.9 (2) |
| O5—Tb1—N5 | 72.69 (6) | N2—C1—C2 | 118.0 (2) |
| O7—Tb1—O4 | 86.19 (7) | C1—C2—H2A | 109.5 |
| O7—Tb1—O5 | 70.93 (6) | C1—C2—H2B | 109.5 |
| O7—Tb1—N1 | 71.68 (6) | C1—C2—H2C | 109.5 |
| O7—Tb1—N3 | 77.33 (6) | H2A—C2—H2B | 109.5 |
| O7—Tb1—N5 | 137.71 (5) | H2A—C2—H2C | 109.5 |
| N3—Tb1—N1 | 79.81 (7) | H2B—C2—H2C | 109.5 |
| N5—Tb1—N1 | 121.66 (6) | O2—C3—N4 | 121.3 (2) |
| N5—Tb1—N3 | 140.98 (6) | O2—C3—C4 | 122.1 (2) |
| C1—O1—Tb1 | 125.30 (14) | N4—C3—C4 | 116.64 (19) |
| C3—O2—Tb1 | 123.84 (14) | C3—C4—H4A | 109.5 |
| C5—O3—Tb1 | 121.19 (13) | C3—C4—H4B | 109.5 |
| N7—O4—Tb1 | 96.95 (15) | C3—C4—H4C | 109.5 |
| N7—O5—Tb1 | 96.06 (14) | H4A—C4—H4B | 109.5 |
| N8—O7—Tb1 | 136.41 (13) | H4A—C4—H4C | 109.5 |
| Tb1—N1—H1A | 111.2 (19) | H4B—C4—H4C | 109.5 |
| Tb1—N1—H1B | 108 (2) | O3—C5—N6 | 121.60 (19) |
| H1A—N1—H1B | 108 (3) | O3—C5—C6 | 121.0 (2) |
| N2—N1—Tb1 | 112.25 (13) | N6—C5—C6 | 117.39 (19) |
| N2—N1—H1A | 109.1 (19) | C5—C6—H6A | 109.5 |
| N2—N1—H1B | 108 (2) | C5—C6—H6B | 109.5 |
| N1—N2—H2 | 119 (2) | C5—C6—H6C | 109.5 |
| C1—N2—N1 | 117.60 (18) | H6A—C6—H6B | 109.5 |
| C1—N2—H2 | 122 (2) | H6A—C6—H6C | 109.5 |
| Tb1—N3—H3A | 111.3 (19) | H6B—C6—H6C | 109.5 |
| Tb1—N3—H3B | 110 (2) | ||
| Tb1—O1—C1—N2 | 3.9 (3) | Tb1—O7—N8—O9 | 178.18 (15) |
| Tb1—O1—C1—C2 | −176.58 (17) | Tb1—N1—N2—C1 | 1.4 (2) |
| Tb1—O2—C3—N4 | 8.5 (3) | Tb1—N3—N4—C3 | 0.0 (3) |
| Tb1—O2—C3—C4 | −171.10 (16) | Tb1—N5—N6—C5 | −6.9 (2) |
| Tb1—O3—C5—N6 | 14.8 (3) | N1—N2—C1—O1 | −3.4 (3) |
| Tb1—O3—C5—C6 | −164.56 (17) | N1—N2—C1—C2 | 177.1 (2) |
| Tb1—O4—N7—O5 | −4.1 (2) | N3—N4—C3—O2 | −5.3 (3) |
| Tb1—O4—N7—O6 | 174.7 (2) | N3—N4—C3—C4 | 174.4 (2) |
| Tb1—O5—N7—O4 | 4.0 (2) | N5—N6—C5—O3 | −4.1 (3) |
| Tb1—O5—N7—O6 | −174.7 (2) | N5—N6—C5—C6 | 175.3 (2) |
| Tb1—O7—N8—O8 | −0.5 (3) |