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. 2022 Mar 15;12(14):8345–8360. doi: 10.1039/d1ra08312k

Experimental parameters for the data acquisition for the NMR experiments.

COSY 13C-HSQC HMBC NOESY 1H 13C-HSQC-AP
Relaxation delay [s] 1 1.5 1 6 1 1.5
Number of transients 4 2 4 4 8 4
Acquisition time [s] 0.15 0.15 0.15 0.15 1.7 1.2
Number of increments 200 300 200 200 n.a. 400