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. 2022 Apr 12;13:1951. doi: 10.1038/s41467-022-29149-z

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© The Author(s) 2022

Open Access This article is licensed under a Creative Commons Attribution 4.0 International License, which permits use, sharing, adaptation, distribution and reproduction in any medium or format, as long as you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons license, and indicate if changes were made. The images or other third party material in this article are included in the article’s Creative Commons license, unless indicated otherwise in a credit line to the material. If material is not included in the article’s Creative Commons license and your intended use is not permitted by statutory regulation or exceeds the permitted use, you will need to obtain permission directly from the copyright holder. To view a copy of this license, visit http://creativecommons.org/licenses/by/4.0/.

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Fig. 4 — a–c Contour plots of in situ PXRD data recorded in parallel to adsorption of MP at 300 K (gray) (a), at 300 K with 365 nm irradiation (blue) (b) and at 296 K (red) (c) and corresponding evolution of peak intensity of the (111) reflection of DUT-163op (open squares) and (E)-DUT-163cp (filled triangles) at 3.1° and 4.02°, respectively (d). e, f Selected PXRD patterns and magnified wide angle region as inset before (middle bottom) and after (middle top) structural contraction at 299 K upon irradiation with 365 nm (e) and at 295 K without irradiation (f) in comparison to simulated PXRD patterns and peak positions for DUT-163op (purple) and (E)-DUT-163cp (orange).