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. 2022 Apr 12;13:1951. doi: 10.1038/s41467-022-29149-z

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© The Author(s) 2022

Open Access This article is licensed under a Creative Commons Attribution 4.0 International License, which permits use, sharing, adaptation, distribution and reproduction in any medium or format, as long as you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons license, and indicate if changes were made. The images or other third party material in this article are included in the article’s Creative Commons license, unless indicated otherwise in a credit line to the material. If material is not included in the article’s Creative Commons license and your intended use is not permitted by statutory regulation or exceeds the permitted use, you will need to obtain permission directly from the copyright holder. To view a copy of this license, visit http://creativecommons.org/licenses/by/4.0/.

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Fig. 5 — a–e Axial PXRD (a) and Raman scan (b) of a capillary with a diameter of 0.7 mm, image and illustration of the investigated capillary (c), selected PXRD patterns at 1 mm (bottom), 6 mm (middle), and 13 mm (top) (d), Raman spectra at selected positions (e), f–h PXRD patterns of non-irradiated and irradiated areas for capillaries with diameters of 0.3 mm (f), 0.7 mm (g), and 1 mm (h). Irradiated regions are marked in orange, non-irradiated areas in purple, inset enlarged patterns in f–h of 2Theta range 3.8-9° represent 20 times magnification.