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. Author manuscript; available in PMC: 2022 Oct 15.
Published in final edited form as: ACS Catal. 2021 Sep 23;11(20):12417–12422. doi: 10.1021/acscatal.1c03113

Table 2.

Scope and limitations with regards to the nitroarene.

graphic file with name nihms-1792124-t0003.jpg
entry R1 R2 R3 3 yield, %a
1 MeO2C H H a 83 (81)b
2 F3C H H b 84
3 H H H c 66
4 Cl H H d 85
5 MeO H H e n.r.
6 O2N H H f 59
7 H F3C H g 89
8 H Me H h 73
9 H MeO H i 85
10 H H NC j 83
11 H H Br k 89
12 H H Et l 82
13 H H OMe m 72
14 −HC=CH−CH=CH− H n 96
15 graphic file with name nihms-1792124-t0004.jpg o 75
a

Isolated after silica gel chromatography.

b

1 mmol reaction scale.