Table 1.

¹H and ¹³C NMR (CD₃OD) data for new adipostatins 9 and 11 in CD₃OD.

Pos.	Adipostatin K (9)		Adipostatin L (11)
	δC	δH (mult., J (Hz))	δC	δH (mult., J (Hz))
1	159.3	−	159.3	−
2	100.9	6.07 (t, 2.2)	101.4	6.11 (t, 2.2)
3	159.3	−	159.3	−
4	107.9	6.12 (d, 2.2)	108.9	6.16 (d, 2.2)
5	146.3	−	142.7	−
6	107.9	6.12 (d, 2.2)	108.9	6.16 (d, 2.2)
1′	37.0	2.44 (t, 7.7)	45.3	2.53 (dd, 13.4, 6.4)2.59 (dd, 13.4,7.0)
2′	32.5	1.58 (m)	73.6	3.72 (m)
3′	30.0–30.8	1.25–1.37	37.7	1.36 (m), 1.50 (m)
4′	30.0–30.8	1.25–1.37	26.8	1.34 (m), 1.48 (m)
5′	30.0–30.8	1.25–1.37	30.0–30.9	1.25–1.37
6′	30.0–30.8	1.25–1.37	30.0–30.9	1.25–1.37
7′	30.0–30.8	1.25–1.37	30.0–30.9	1.25–1.37
8′	28.1	2.03 (m)	30.0–30.9	1.25–1.37
9′	130.8	5.34 (t, 4.9)	28.1	2.03 (m)
10′	130.8	5.34 (t, 4.9)	130.8	5.34 (td, 4.6, 2.2)
11′	28.1	2.03 (m)	130.8	5.34 (td, 4.6, 2.2)
12′	30.0–30.8	1.25–1.37	28.1	2.03 (m)
13′	30.0–30.8	1.25–1.37	30.0–30.9	1.25–1.37
14′	32.9	1.25–1.37	30.0–30.9	1.25–1.37
15′	23.7	1.25–1.37	32.9	1.25–1.37
16′	14.4	0.91 (t, 6.7)	23.7	1.25–1.37
17′			14.4	0.89 (t, 6.7)