Table 2.

¹H (700 MHz), ¹³C (175 MHz), HMBC, COSY, and ROESY NMR data for compound 11 (δ in ppm, J in Hz, CDCL₃).

Position	13C	1H	HMBC	COSY	ROESY
1	194.7
2	194.6
3	109.1
4	158.9
5	115.3
6	152.5
7	136.8
8	113.7	6.84, s, 1H	C-2, 4, 6, 7		OH-7
1′	111.1
2′	165.2
3′	104.3	6.44, s, 1H	C-1′, 2′, 4′, 5′
4′	163.7
5′	119.9
6′	133.9	7.18, s, 1H	C-1, 1′, 2′, 5′, 1‴		H-1‴
1″	22.0	3.51, d, J = 7.3, 2H	C-4, 5, 6, 2″, 3″	H-2″, 9″	H-2″, 9″, OH-6
2″	120.5	5.33, t, J = 7.3, 1H	C-1″	H-1″, 9″	H-1″, 4″, OH-6
3″	139.7
4″	39.7	2.09, m, 2H	C-2″, 3″, 5″, 6″		H-2″, 6″
5″	26.4	2.13, m, 2H	C-3″, 6″, 7″	H-6″	H-6″
6″	123.8	5.07, m, 1H		H-5″, 8″, 10″	H-4″, 5″
7″	132.1
8″	25.7	1.68, s, 3H	C-6″, 7″, 10″	H-6″
9″	16.3	1.84, s, 3H	C-2″, 3″, 4″	H-1″, 2″	H-1″
10″	17.7	1.60, s, 3H	C-6″, 7″, 8″	H-6″
1‴	29.1	3.23, d, J = 7.2, 2H	C-4′, 5′, 6′, 2‴, 3‴	H-2‴, 4‴, 5‴	H-2‴, 4‴, 5‴, 6′, OH-4′
2‴	120.8	5.20, t, J = 7.2, 2H		H-1‴, 4‴, 5‴	H-1‴, 5‴
3‴	136.4
4‴	25.7	1.73, s, 3H	C-2‴, 3‴, 5‴	H-1‴, 2‴	H-1‴
5‴	17.9	1.71, s, 3H	C-2‴, 3‴, 4‴	H-1‴, 2‴	H-1‴, 2‴
OH-4		11.92, s, 1H	C-3, 4, 5
OH-6		6.68, s, 1H	C-5, 6, 7		H-2″, 1″, OH-7
OH-7		5.05, bs, 1H			H-8, OH-6
OH-2′		11.59, s, 1H	C1′, 2′, 3′, 4′
OH-4′		6.11, s, 1H	C-3′, 4′, 5′		H-1‴