| Crystal data |
| Chemical formula |
[Cu(C9H6N3O2)2(C2H7N)2] |
|
M
r
|
530.06 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
293 |
|
a, b, c (Å) |
6.3657 (5), 8.1428 (7), 12.1896 (11) |
| α, β, γ (°) |
72.595 (2), 89.376 (2), 87.805 (2) |
|
V (Å3) |
602.47 (9) |
|
Z
|
1 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
0.95 |
| Crystal size (mm) |
0.36 × 0.32 × 0.27 |
| |
| Data collection |
| Diffractometer |
Bruker SMART CCD |
| Absorption correction |
Multi-scan (SADABS; Bruker, 2002 ▸) |
|
T
min, T
max
|
0.727, 0.785 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
3971, 2727, 2345 |
|
R
int
|
0.017 |
| (sin θ/λ)max (Å−1) |
0.650 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.038, 0.093, 1.03 |
| No. of reflections |
2727 |
| No. of parameters |
160 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
0.28, −0.20 |
