A comparison of the catalytic activity of the (Fe3O4@NFC@NSalophCu)CO2H catalyst with some reported catalysts for 5-substituted-1H-tetrazole multi-component reactions.
Reaction | Catalyst | Reaction conditions | Time (h) | Yielda (%) | Ref. |
---|---|---|---|---|---|
5-Substituted-1H-tetrazoleb | CuNO3·3H2O | DMSO/120 °C | 24 | 78 | 65 |
Nano-Cu2O-MFR | DMF/100 °C | 8 | 92 | 66 | |
Cu–MCM-41 | DMF/140 °C | 12 | 90 | 67 | |
Copper(ii) Schiff base | DMF/110 °C | 7 | 91 | 53 | |
Bi(OTf)3 | DMF/120 °C | 24 | 87 | 68 | |
Cu(OAC)2 | DMF/120 °C | 12 | 96 | 69 | |
(NH4)4Ce(SO4)4–2H2O | DMF/reflux | 5 | 72 | 70 | |
Humic acid | H2O/100 °C | 4 | 92 | 71 | |
Fe3O4–CNT–TEA–Cu(ii) | DMF/70 °C | 1.5 | 96 | 54 | |
(Fe3O4@NFC@NSalophCu)CO2H | H2O/60 °C | 0.25 | 97 | This work |
Isolated yield.
Reaction conditions: benzaldehyde (1.0 mmol), hydroxylamine (1.2 mmol), and sodium azide (1.5 mmol).