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. 2021 Jun 15;11(34):21153–21169. doi: 10.1039/d1ra03276c

1H and 13C NMR data (400 MHz for 1H, and 100 MHz for 13C) of compound 10a.

Position 10b
δ H δ C
1 129.8
2 7.06 s 110.1
3 145.0
4 141.9
4a 117.1
4b 127.3
5 8.80 d (9.2) 123.7
6 7.28 d (9.2) 112.7
7 149.9
8 143.2
8a 123.6
9 7.92 d (9.6) 118.6
10 7.81 d (9.6) 122.9
10a 125.1
11 3.29 m 31.4
12 3.14 m 61.9
OCH2O 6.19 s 100.9
7-OCH3 4.00 s 56.3
8-OCH3 3.98 s 61.2
N–CH3 2.81 s 46.9
graphic file with name d1ra03276c-t11.jpg 2.09 s 19.5
graphic file with name d1ra03276c-t12.jpg 169.7
a

Assignments were based on 1H–1H COSY, HMQC, HMBC, and NOESY experiments; chemical shifts (δ) are given in ppm.

b

Recorded in CDCl3.