2 |
165.5, C |
|
168.4, C |
|
3 |
113.1, CH |
6.10 (1H, s) |
112.5, CH |
6.09, s |
4 |
177.5, C |
|
177.6, C |
|
4a |
122.2, C |
|
122.4, C |
|
5 |
60.0, CH |
4.73, dd, (4.2, 4.2, 3.6) |
60.0, CH |
4.74, ddd, (4.2, 3.6, 3.6) |
6 |
39.2, CH2
|
1.89, ddd, (12.6, 3.6, 3.6) |
39.4, CH2
|
1.89, ddd, (12.6, 3.6, 3.6) |
1.52, ddd, (12.6, 10.8, 4.2) |
1.53, ddd, (12.6, 10.8, 3.6) |
7 |
61.1, CH |
4.14, (m) |
61.1, CH |
4.13, m |
8 |
36.3, CH2
|
2.80, dd, (17.4, 5.4) |
36.3, CH2
|
2.80, dd, (17.4, 6.0) |
2.38, ddd, (17.4, 9.0) |
2.39, dd, (17.4, 9.0) |
8a |
162.6, C |
|
162.7, C |
|
9 |
19.2, CH3
|
2.22, s |
34.4, CH2
|
2.46, t, (7.2) |
10 |
|
|
19.7, CH2
|
1.60, m |
11 |
|
|
13.2, CH3
|
0.91, t, (7.2) |
5-OH |
|
4.84, d, (4.2) |
|
4.84, d, (4.2) |
7-OH |
|
5.03, d, (4.2) |
|
5.02, d, (4.8) |