Skip to main content
. 2021 Jun 29;11(36):22489–22494. doi: 10.1039/d1ra03754d

1H (600 MHz) and 13C NMR (150 MHz) data of compounds 9 and 10 in DMSO-d6.

No. 9 10
δ C δ H (J in Hz) δ C δ H (J in Hz)
2 165.5, C 168.4, C
3 113.1, CH 6.10 (1H, s) 112.5, CH 6.09, s
4 177.5, C 177.6, C
4a 122.2, C 122.4, C
5 60.0, CH 4.73, dd, (4.2, 4.2, 3.6) 60.0, CH 4.74, ddd, (4.2, 3.6, 3.6)
6 39.2, CH2 1.89, ddd, (12.6, 3.6, 3.6) 39.4, CH2 1.89, ddd, (12.6, 3.6, 3.6)
1.52, ddd, (12.6, 10.8, 4.2) 1.53, ddd, (12.6, 10.8, 3.6)
7 61.1, CH 4.14, (m) 61.1, CH 4.13, m
8 36.3, CH2 2.80, dd, (17.4, 5.4) 36.3, CH2 2.80, dd, (17.4, 6.0)
2.38, ddd, (17.4, 9.0) 2.39, dd, (17.4, 9.0)
8a 162.6, C 162.7, C
9 19.2, CH3 2.22, s 34.4, CH2 2.46, t, (7.2)
10 19.7, CH2 1.60, m
11 13.2, CH3 0.91, t, (7.2)
5-OH 4.84, d, (4.2) 4.84, d, (4.2)
7-OH 5.03, d, (4.2) 5.02, d, (4.8)