Fig. 15. Monitoring the Suzuki coupling reaction of 4-iodoanisole with phenylboronic acid catalyzed by 5-Pd. Reaction conditions: phenylboronic acid (0.05 mmol), 4-iodoanisole (0.05 mmol), K2CO3 (0.15 mmol), cis-5-Pd catalyst solution (DMF/H2O 1 : 1, 0.755 mL, 0.6 mol% Pd), DMF/H2O 1 : 1 (2.245 mL), λmax = 365 nm (continuous irradiation), P = 30 W.
