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. 2021 Jul 9;11(38):23419–23429. doi: 10.1039/d1ra03838a

Comparison of selected bond lengths and bond angles of 5-Pd and a related complex (“literature”) previously reported in the literature25.

graphic file with name d1ra03838a-u1.jpg
Bond length (Å) (5-Pd) Bond length (Å) (lit) Bond angle (°) (5-Pd) Bond angle (°) (lit)
Pd–Cl1 2.285 2.285 N1–Pd–N2 80.26 80.6
Pd–Cl2 2.289 2.264 N1–Pd–Cl1 93.83 94.0
Pd–N1 2.050 2.055 N2–Pd–Cl2 94.79 94.4
Pd–N2 2.005 2.007 Cl1–Pd–Cl2 91.08 91.01
N1–C5 1.353 n.d.
C5–C6 1.453 1.464
C6–C7 1.363 1.359
C7–N4 1.338 1.343
N4–N3 1.345 1.349
N3–N2 1.294 1.312
N2–C6 1.374 1.364