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. 2022 Mar 16;85(4):910–916. doi: 10.1021/acs.jnatprod.1c01024

Table 2. 13C NMR Data (200 MHz) of Compounds 14 in CDCl3.

  δC, type
atom# 1 2 3 4
1 40.1, CH2 40.1, CH2 41.0, CH2 41.1, CH2
2 70.3, CH 69.9, CH 71.2, CH 70.7, CH
3 79.0, CH 78.9, CH 80.1, CH 80.0, CH
4 39.3, C 39.2, C 39.3, C 39.3, C
5 49.3, CH 49.3, CH 49.9, CH 50.0, CH
6 36.2, CH2 36.2, CH2 17.9, CH2 17.9, CH2
7 197.8, C 197.8, C 25.8, CH2 25.9, CH2
8 139.2, C 139.1, C 134.8, C 134.7, C
9 163.1, C 163.0, C 134.2, C 134.2, C
10 40.5, C 40.5, C 37.8, C 37.9, C
11 23.8, CH2 23.8, CH2 33.8, CH2 34.0, CH2
12 29.9, CH2 29.9, CH2 72.8, CH2 72.8, CH2
13 44.9, C 44.9, C 49.0, C 49.0, C
14 47.8, C 47.8, C 52.2, C 52.2, C
15 31.8, CH2 31.8, CH2 31.2, CH2 31.1, CH2
16 28.6, CH2 28.6, CH2 25.1, CH2 25.2, CH2
17 48.9, CH 48.9, CH 50.5, CH 50.6, CH
18 15.8, CH3 15.7, CH3 9.9, CH3 9.8, CH3
19 19.4, CH3 19.4, CH3 20.0, CH3 20.0, CH3
20 35.9, CH 35.9, CH 33.8, CH 33.8, CH
21 18.5, CH3 18.5, CH3 21.2, CH3 21.2, CH3
22 30.1, CH2 30.0, CH2 29.1, CH2 29.1, CH2
23 32.6, CH2 32.5, CH2 33.7, CH2 33.6, CH2
24 214.9, C 214.8, C 215.2, C 215.1, C
25 76.2, C 76.2, C 76.3, C 76.2, C
26 26.5, CH3 26.6, CH3 26.5, CH3 26.5, CH3
27 26.5, CH3 26.5, CH3 26.5, CH3 26.5, CH3
28 25.0, CH3 25.0, CH3 24.2, CH3 24.1, CH3
29 17.3, CH3 17.2, CH3 17.4, CH3 17.4, CH3
30 27.6, CH3 27.6, CH3 28.2, CH3 28.2, CH3
1′ 170.8, C 171.2, C 171.5, C 171.4, C
2′ 44.9, CH2 44.8, CH2 44.7, CH2 44.9, CH2
3′ 69.6, C 69.5, C 69.7, C 69.5, C
4′ 27.1, CH3 27.3, CH3 27.2, CH3 26.5, CH3
5′ 44.8, CH2 44.7, CH2 45.0, CH2 44.7, CH2
6′ 173.7, C 172.1, C 173.5, C 172.1, C
7′   51.7, CH3   51.7, CH3
3-OAc 171.4, C 170.6, C 171.1, C 170.8, C
  20.9, CH3 20.9, CH3 21.0, CH3 21.0, CH3