Table 3. 13C (175 MHz) NMR Data of Compounds 6–8 in CDCl3.
6 | 7 | 8 | |
---|---|---|---|
position | δC, type | δC, type | δC, type |
1 | 71.7, C | 70.9, C | 150.3, C |
2 | 80.1, CH | 76.5, CH | 73.0, CH |
3 | 36.8, CH | 121.9, C | 48.0, CH |
4 | 40.2, CH | 144.7, C | 46.6, CH |
5 | 27.2, CH2 | 27.5, CH2 | 34.0, CH2 |
6 | 33.0, CH2 | 29.2, CH2 | 33.9, CH2 |
7 | 27.5, CH3 | 26.1, CH3 | 104.7, CH2 |
8 | 147.8, C | 148.9, C | 147.8, C |
9 | 110.8, CH2 | 113.5, CH2 | 110.4, CH2 |
10 | 18.2, CH3 | 21.3, CH3 | 19.05, CH3 |
1′ | 153.0, C | 153.9, C | 155.0, C |
2′ | 107.4, CH | 107.8, CH | 109.0, CH |
3′ | 143.2, C | 144.9, C | 143.0, C |
4′ | 110.9, CH | 107.1, CH | 108.7, CH |
5′ | 157.6, C | 153.0, C | 154.7, C |
6′ | 112.5, C | 113.4, C | 110.7, C |
1″ | 35.2, CH2 | 35.9, CH2 | 35.2, CH2 |
2″ | 27.4, CH2 | 27.4, CH2 | 27.4, CH2 |
3″ | 31.3, CH2 | 30.4, CH2 | 31.3, CH2 |
4″ | 22.3, CH2 | 22.3, CH2 | 22.3, CH2 |
5″ | 14.0, CH3 | 14.0, CH3 | 14.0, CH3 |